Evaluation of various digestion procedures for trace element contents of some food materials

被引：123

作者：

Demirel, Sule ^{[2
]}

Tuzen, Mustafa ^{[2
]}

Saracoglu, Sibel ^{[1
]}

Soylak, Mustafa ^{[3
]}

机构：

[1] Erciyes Univ, Fac Educ, TR-38039 Kayseri, Turkey

[2] Gaziosmanpasa Univ, Fac Sci & Arts, Dept Chem, TR-60250 Tokat, Turkey

[3] Erciyes Univ, Fac Art & Sci, Dept Chem, TR-38039 Kayseri, Turkey

来源：

JOURNAL OF HAZARDOUS MATERIALS | 2008年 / 152卷 / 03期

关键词：

trace elements; dry ashing; wet ashing; microwave digestion; food samples;

D O I：

10.1016/j.jhazmat.2007.07.077

中图分类号：

X [环境科学、安全科学];

学科分类号：

08 [工学]; 0830 [环境科学与工程];

摘要：

The levels of trace elements in different types of food material consumed in Turkey were determined by flame and graphite furnace atomic absorption spectrometry. Food samples were digested with dry ashing, wet ashing and microwave digestion procedures in this study. The microwave digestion procedure was chosen for the digestion of all the food samples because it required shorter time and made higher recovery (specially for Se). Fe, Cu, Mn, Zn, Al and Se were determined by flame and graphite furnace atomic absorption spectrometry, respectively. Relative standard deviations (RSD) were found below 10%. The accuracy of the procedure was confirmed by certified reference materials. Moreover, this procedure was easier to use when compared with dry and wet digestions. (C) 2007 Elsevier B.V. All rights reserved.

引用

页码：1020 / 1026

页数：7

共 41 条

[1]

Heavy metals in edible green vegetables grown along the sites of the Sinza and Msimbazi rivers in Dar es Salaam, Tanzania [J].

Bahemuka, TE ;

Mubofu, EB .

FOOD CHEMISTRY, 1999, 66 (01) :63-66

[2]

Borkowska-Burnecka J, 2000, CHEM ANAL-WARSAW, V45, P429

[3]

Bloavailability of heavy metals from polluted soils to plants [J].

Chojnacka, K ;

Chojnacki, A ;

Górecka, H ;

Górecki, H .

SCIENCE OF THE TOTAL ENVIRONMENT, 2005, 337 (1-3) :175-182

[4]

A comparison of sample preparation procedures for the determination of iron and zinc in bulgur wheat by graphite furnace atomic absorption spectrometry [J].

Doner, G ;

Akman, S .

ANALYTICAL LETTERS, 2000, 33 (15) :3333-3341

[5]

Speciation of aluminum in tea infusion by ion-exchange resins and flame AAS detection [J].

Erdemoglu, SB ;

Pyrzyniska, K ;

Güçer, S .

ANALYTICA CHIMICA ACTA, 2000, 411 (1-2) :81-89

[6]

Multi-element analysis of tea beverages by inductively coupled plasma atomic emission spectrometry [J].

Fernández, PL ;

Pablos, F ;

Martín, MJ ;

González, AG .

FOOD CHEMISTRY, 2002, 76 (04) :483-489

[7]

Selenium in health and disease: A review [J].

Foster, LH ;

Sumar, S .

CRITICAL REVIEWS IN FOOD SCIENCE AND NUTRITION, 1997, 37 (03) :211-228

[8]

Simultaneous preconcentration and determination of copper, nickel, cobalt and lead ions content by flame atomic absorption spectrometry [J].

Ghaedi, Mehrorang ;

Ahmadi, Farshid ;

Shokrollahi, Ardeshir .

JOURNAL OF HAZARDOUS MATERIALS, 2007, 142 (1-2) :272-278

[9]

*HLTH CAN, 2004, TRAC MET AN INF FORM

[10]

Determination of selenium in garlic by cathodic stripping voltammetry [J].

Inam, R ;

Somer, G .

FOOD CHEMISTRY, 1999, 66 (03) :381-385

← 1 2 3 4 5 →