Aging time effect on the synthesis of small crystal LTA zeolites in the absence of organic template

被引:71
作者
Alfaro, S. [1 ]
Rodriguez, C.
Valenzuela, M. A.
Bosch, P.
机构
[1] Inst Politecn Nacl, ESIQIE, Lab Catalisis & Mat, Mexico City 07738, DF, Mexico
[2] Univ Nacl Autonoma Mexico, Inst Invest Mat, Mexico City 04510, DF, Mexico
关键词
crystal growth; nanomaterials; hydrothermal synthesis; zeolite LTA; aging time;
D O I
10.1016/j.matlet.2007.03.009
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Crystals of LTA zeolites were obtained in absence of organic templates using a crystallization temperature of 373 K. The as-synthesized samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), and Fourier-Transform Infrared (FTIR) spectroscopy. The aging time was found to be a crucial factor for the control of the crystal size. Samples aged between 72 and 144 h presented an average crystal size of ca. 200 to 500 nm. (c) 2007 Elsevier BY. All rights reserved.
引用
收藏
页码:4655 / 4658
页数:4
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