Synthesis of carbon micro-spheres by a glucose hydrothermal method

被引:194
作者
Mi, Yuanzhu [1 ,2 ]
Hu, Weibing [1 ]
Dan, Youmeng [1 ]
Liu, Yingliang [3 ]
机构
[1] Hubei Inst Nationalities, Sch Chem & Environm Engn, Enshi 445000, Peoples R China
[2] Yangtze Univ, Sch Chem & Environm Engn, Jinzhou 434023, Peoples R China
[3] Jinan Univ, Dept Chem, Guangzhou 510632, Guangdong, Peoples R China
关键词
characterization methods; composite materials;
D O I
10.1016/j.matlet.2007.08.011
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Carbon micro-spheres with a regular and perfect shape, high yields and narrow size distribution were successfully synthesized by a hydrothermal route in a stainless steel autoclave. In this process, the aqueous glucose solution was used as starting materials. The optimal reaction conditions for obtaining carbon micro-spheres were 500 degrees C and 12 h. The resulting products were characterized by using combined techniques including X-ray powder diffractometer (XRD), scanning electron microscopy (SEM), energy-dispersive X-ray spectrometer (EDX) and Raman spectroscopy. The diameters of carbon micro-spheres ranged from I to 2 gin. (C) 2007 Elsevier B.V. All rights reserved.
引用
收藏
页码:1194 / 1196
页数:3
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