Ultrasound assisted additive free synthesis of nanocrystalline zinc oxide

被引：32

作者：

Bhatte, Kushal D. ^{[1
]}

Fujita, Shin-Ichiro ^{[2
]}

Arai, Masahiko ^{[2
]}

Pandit, Anirudha B. ^{[3
]}

Bhanage, Bhalchandra M. ^{[1
]}

机构：

[1] Inst Chem Technol Autonomous, Dept Chem, Bombay 400019, Maharashtra, India

[2] Hokkaido Univ, Grad Sch Engn, Div Chem Proc Engn, Sapporo, Hokkaido 0608628, Japan

[3] Inst Chem Technol Autonomous, Dept Chem Engn, Bombay 400019, Maharashtra, India

来源：

ULTRASONICS SONOCHEMISTRY | 2011年 / 18卷 / 01期

关键词：

Nanocrystalline; ZnO; Ultrasound; 1,4-Butanediol; ZNO NANOPARTICLES; GROWTH; SONOLUMINESCENCE;

D O I：

10.1016/j.ultsonch.2010.06.001

中图分类号：

O42 [声学];

学科分类号：

070206 ; 082403 ;

摘要：

A novel method for the synthesis of nanocrystalline zinc oxide without any additive was developed using zinc acetate and 1,4-butanediol through sonication. The structure and morphology of prepared nanocrystalline zinc oxide was investigated by various techniques like TEM. XRD, EDAX, UV-Vis spectroscopy. The solvent 1,4-butanediol played a dual role of fuel as well as capping agent eliminating addition of any extraneous species. The results showed that using ultrasound sonication is green, cost effective compared to conventional wet chemical method for ZnO nanoparticle synthesis. (C) 2010 Elsevier B.V. All rights reserved.

引用

页码：54 / 58

页数：5

共 17 条

[1] Photoresponse of sol-gel-synthesized ZnO nanorods [J].

Ahn, SE ;

Lee, JS ;

Kim, H ;

Kim, S ;

Kang, BH ;

Kim, KH ;

Kim, GT .

APPLIED PHYSICS LETTERS, 2004, 84 (24) :5022-5024

[2] Solvothermal synthesis of ZnO with various aspect ratios using organic solvents [J].

Ayudhya, Sirachaya Kunjara Na ;

Tonto, Parawee ;

Mekasuwandumrong, Okorn ;

Pavarajarn, Varong ;

Praserthdam, Piyasan .

CRYSTAL GROWTH & DESIGN, 2006, 6 (11) :2446-2450

[3] From ZnO nanorods to nanoplates: Chemical bath deposition growth and surface-related emissions [J].

Cao, Bingqiang ;

Cai, Weiping .

JOURNAL OF PHYSICAL CHEMISTRY C, 2008, 112 (03) :680-685

[4] Synthesis and optical properties of tetrapod-like zinc oxide nanorods [J].

Dai, Y ;

Zhang, Y ;

Li, QK ;

Nan, CW .

CHEMICAL PHYSICS LETTERS, 2002, 358 (1-2) :83-86

[5] A facile method to fabricate ZnO hollow spheres and their photocatalytic property [J].

Deng, Ziwei ;

Chen, Min ;

Gu, Guangxin ;

Wu, Limin .

JOURNAL OF PHYSICAL CHEMISTRY B, 2008, 112 (01) :16-22

[6] THE TEMPERATURE OF CAVITATION [J].

FLINT, EB ;

SUSLICK, KS .

SCIENCE, 1991, 253 (5026) :1397-1399

[7] Microwave-assisted synthesis and characterization of flower shaped zinc oxide nanostructures [J].

Krishnakumar, T. ;

Jayaprakash, R. ;

Pinna, Nicola ;

Singh, V. N. ;

Mehta, B. R. ;

Phani, A. R. .

MATERIALS LETTERS, 2009, 63 (02) :242-245

[8] Direct synthesis of monodispersed ZnO nanoparticles in an aqueous solution [J].

Li, Minggang ;

Hari-Bala ;

Lv, Xiaotang ;

Ma, Xiaokun ;

Sun, Fang ;

Tang, Lanqin ;

Wang, Zichen .

MATERIALS LETTERS, 2007, 61 (03) :690-693

[9] Sonoluminescence temperatures during multi-bubble cavitation [J].

McNamara, WB ;

Didenko, YT ;

Suslick, KS .

NATURE, 1999, 401 (6755) :772-775

[10] Sonochemistry and sonoluminescence of room-temperature ionic liquids [J].

Oxley, JD ;

Prozorov, T ;

Suslick, KS .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2003, 125 (37) :11138-11139

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