Gamma ray spectrometers fabricated from Modified Bridgman annealed CZT crystal material

被引:7
作者
Chattopadhyay, K [1 ]
Chen, H [1 ]
Chen, KT [1 ]
Burger, A [1 ]
Flint, JP [1 ]
Glass, HL [1 ]
James, RB [1 ]
机构
[1] Fisk Univ, Ctr Photon Mat & Devices, Nashville, TN 37208 USA
来源
SEMICONDUCTORS FOR ROOM-TEMPERATURE RADIATION DETECTOR APPLICATIONS II | 1997年 / 487卷
关键词
D O I
10.1557/PROC-487-123
中图分类号
TM [电工技术]; TN [电子技术、通信技术];
学科分类号
0808 ; 0809 ;
摘要
The CZT boule was grown by a modified Vertical Bridgman process using in-situ compounding, Cd over-pressure and a pyrolytic boron nitride crucible within a fused ampoule. During growth, the Cd vapor pressure was near 1 atmosphere. These growth conditions tend to give high purity, good stoichiometry, few precipitates, and dislocation densities in the low to mid-10(4) cm(-2) range. The crystals, after polishing, were annealed in a nearly saturated Cd, Zn atmosphere to fill residual Cd-site vacancies and achieve high resistivity in the 10(10) Omega-cm range. Low temperature photoluminescence study shows very good crystalline quality and a very low concentration of deep level recombinations. Single crystal samples were diced into 1 cm squares for evaluation as gamma ray detectors. The best detector results (4.5 % resolution at 60 keV) were achieved for a 2 hour anneal at 850 degrees C.
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页码:123 / 128
页数:6
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