(C6H16N2)2[Mo8O26]:: a new β-octamolybdate salt

被引:10
作者
Muller, EA
Sarjeant, AN
Norquist, AJ
机构
[1] Haverford Coll, Dept Chem, Haverford, PA 19041 USA
[2] Johns Hopkins Univ, Dept Chem, Baltimore, MD 21218 USA
来源
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2005年 / 61卷
关键词
D O I
10.1107/S1600536805008330
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
Crystals of the title compound, 2,5-dimethylpiperazinediium beta-octamolybdate, were grown under mild hydrothermal conditions. The anion and cations lie on inversion centers. A network of N - H center dot center dot center dot O bonds helps to stabilize the crystal packing.
引用
收藏
页码:M730 / M732
页数:3
相关论文
共 19 条
[1]   SIR92 - a program for automatic solution of crystal structures by direct methods [J].
ALTOMARE, A ;
CASCARANO, G ;
GIACOVAZZO, G ;
GUAGLIARDI, A ;
BURLA, MC ;
POLIDORI, G ;
CAMALLI, M .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1994, 27 :435-435
[2]   CRYSTALS version 12: software for guided crystal structure analysis [J].
Betteridge, PW ;
Carruthers, JR ;
Cooper, RI ;
Prout, K ;
Watkin, DJ .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2003, 36 :1487-1487
[3]   THE ANALYTICAL CALCULATION OF ABSORPTION IN MULTIFACETED CRYSTALS [J].
CLARK, RC ;
REID, JS .
ACTA CRYSTALLOGRAPHICA SECTION A, 1995, 51 :887-897
[4]  
DOWTY E, 2002, ATOMS VERSION 6 0
[5]   Asymmetric cation coordination in oxide materials:: Influence of lone-pair cations on the intra-octahedral distortion in d0 transition metals [J].
Halasyamani, PS .
CHEMISTRY OF MATERIALS, 2004, 16 (19) :3586-3592
[6]   TETRAKIS(TETRAMETHYLAMMONIUM) OCTAMOLYBDATE DIHYDRATE [J].
HARRISON, WTA ;
STUCKY, GD ;
GIER, TE .
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1993, 49 :1900-1902
[7]   DERIVATIZED POLYOXOMOLYBDATES - SYNTHESIS AND CHARACTERIZATION OF OXOMOLYBDATE CLUSTERS CONTAINING COORDINATIVELY BOUND DIAZENIDO UNITS - CRYSTAL AND MOLECULAR-STRUCTURE OF THE OCTANUCLEAR OXOMOLYBDATE (NHET3)2(N-BU4N)8[MO8O20(NNPH)6] AND COMPARISON TO THE STRUCTURES OF THE PARENT OXOMOLYBDATE ALPHA-(N-BU4N)4[MO8O26] AND THE TETRANUCLEAR (DIAZENIDO) OXOMOLYBDATES (N-BU4N)2[MO4O10(OME)2(NNPH)2] AND (N-BU4N)2[MO4O8(OME)2(NNC6H4NO2)4]R [J].
HSIEH, TC ;
SHAIKH, SN ;
ZUBIETA, J .
INORGANIC CHEMISTRY, 1987, 26 (24) :4079-4089
[8]   OUT-OF-CENTER DISTORTIONS AROUND OCTAHEDRALLY COORDINATED D(0) TRANSITION-METALS [J].
KUNZ, M ;
BROWN, ID .
JOURNAL OF SOLID STATE CHEMISTRY, 1995, 115 (02) :395-406
[9]  
LINDQVIST I, 1950, ARK KEMI, V2, P349
[10]   THE 1ST OBSERVATION OF GAMMA-OCTAMOLYBDATE - SYNTHESIS, CRYSTAL AND MOLECULAR-STRUCTURE OF [ME3N(CH2)6NME3]2[MO8O26].2H2O [J].
NIVEN, ML ;
CRUYWAGEN, JJ ;
HEYNS, JBB .
JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1991, (08) :2007-2011