Deposition of alumina coatings on monocrystalline diamonds by sol-gel techniques

被引:21
作者
Felde, B [1 ]
Mehner, A [1 ]
Kohlscheen, J [1 ]
Gläbe, R [1 ]
Hoffmann, F [1 ]
Mayr, P [1 ]
机构
[1] Stiftung Inst Werkstofftechn, D-28359 Bremen, Germany
关键词
adhesion; coating; transmission electron microscopy; hardness;
D O I
10.1016/S0925-9635(00)00490-8
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Machining of steel or iron-based alloys with diamond tools leads to rapid tool failure - probably due to chemical wear. The use of monocrystalline diamond tools has, up to now, been obligatory for precision machining. Coating the diamonds with a thin but hard and chemically inert alumina film may overcome the problem. Alumina coatings were deposited by sol-gel techniques. It was shown that a very thin TiN intermediate layer, deposited by reactive sputtering, results in a good adhesion of the alumina coatings to the monocrystalline diamonds. The microstructure of the coatings was characterized by held-emission scanning electron microscopy (FE-SEM) and by transmission electron microscopy (TEM). The deposited coatings showed a nanocrystalline, dense microstructure. The hardness of the coatings was investigated by ultramicrohardness measurements (UMH). (C) 2001 Elsevier Science B.V. All rights reserved.
引用
收藏
页码:515 / 518
页数:4
相关论文
共 13 条
[1]   DIAMOND COATING OF TITANIUM-ALLOYS [J].
DRORY, MD ;
HUTCHINSON, JW .
SCIENCE, 1994, 263 (5154) :1753-1755
[2]   Adhesion of diamond coatings on steel and copper with a titanium interlayer [J].
Fan, QH ;
Fernandes, A ;
Pereira, E ;
Grácio, J .
DIAMOND AND RELATED MATERIALS, 1999, 8 (8-9) :1549-1554
[3]   WEAR-RESISTANT DIAMOND COATINGS ON ALUMINA [J].
FAN, WD ;
WU, H ;
JAGANNADHAM, K ;
GORAL, BC .
SURFACE & COATINGS TECHNOLOGY, 1995, 72 (1-2) :78-87
[4]  
FELDE B, 1999, P EUR 99 MUNCH 27 30, V11
[5]   Processing and characterization of alumina thin films on chemically vapor deposited diamond substrates for producing adherent metallizations [J].
Menon, ESK ;
Dutta, I .
JOURNAL OF MATERIALS RESEARCH, 1999, 14 (02) :565-577
[6]   SYNTHESIS OF AN ALUMINA COATING FROM CHELATED ALUMINUM ALKOXIDES [J].
NASS, R ;
SCHMIDT, H .
JOURNAL OF NON-CRYSTALLINE SOLIDS, 1990, 121 (1-3) :329-333
[7]   Chemical aspects of tool wear in single point diamond turning [J].
Paul, E ;
Evans, CJ ;
Mangamelli, A ;
McGlauflin, ML ;
Polavani, RS .
PRECISION ENGINEERING-JOURNAL OF THE INTERNATIONAL SOCIETIES FOR PRECISION ENGINEERING AND NANOTECHNOLOGY, 1996, 18 (01) :4-19
[8]   State of the art in hard coatings for carbide cutting tools [J].
Prengel, HG ;
Pfouts, WR ;
Santhanam, AT .
SURFACE & COATINGS TECHNOLOGY, 1998, 102 (03) :183-190
[9]  
Schneider JM, 1997, SURF COAT TECH, V94-5, P179
[10]  
TAMINIAU DA, 1994, P 3 INT C ULTR MAN E, P25