Influence of the extraction mode on the yield of some furanocoumarins from Pastinaca sativa fruits

被引:47
作者
Waksmundzka-Hajnos, M
Petruczynik, A
Dragan, A
Wianowska, D
Dawidowicz, AL
Sowa, I
机构
[1] Med Univ, Dept Inorgan & Analyt Chem, PL-20081 Lublin, Poland
[2] Marie Curie Sklodowska Univ, Fac Chem, Dept Chem Phys & Physicochem Separat Methods, PL-20031 Lublin, Poland
来源
JOURNAL OF CHROMATOGRAPHY B-ANALYTICAL TECHNOLOGIES IN THE BIOMEDICAL AND LIFE SCIENCES | 2004年 / 800卷 / 1-2期
关键词
solid-liquid extraction; microwave-assisted solvent extraction; accelerated solvent extraction; ultrasonification; furanocoumarins;
D O I
10.1016/j.jchromb.2003.07.006
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
Analysis of plant material is an important task in chemotaxonomical investigations, in search of plants with pharmacological activity or in standardisation of plant drugs. The choice of optimal conditions for the analysis of plant material and effect of extraction method on the yield of furanocoumarins from Pastinaca sativa fruits were examined. The following extraction methods were used in experiments: exhaustive extraction in Soxhlet apparatus, ultrasonification (USAE) at 25 and 60degreesC, microwave-assisted solvent extraction in open and closed system (MASE) and accelerated solvent extraction (ASE). In most cases, the yield of furanocoumarins was highest by use of ASE method as well as by ultrasonification at 60degreesC. (C) 2003 Elsevier B.V. All rights reserved.
引用
收藏
页码:181 / 187
页数:7
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