Incidence of patulin in fruits and fruit juices marketed in Campinas, Brazil

被引:53
作者
de Sylos, CM [1 ]
Rodriguez-Amaya, DB [1 ]
机构
[1] Univ Estadual Campinas, Fac Engn Alimentos, Dept Ciencia Alimentos, BR-13081970 Campinas, SP, Brazil
来源
FOOD ADDITIVES AND CONTAMINANTS | 1999年 / 16卷 / 02期
基金
巴西圣保罗研究基金会;
关键词
patulin; contamination; mycotoxin; fruits; fruit juices;
D O I
10.1080/026520399284226
中图分类号
O69 [应用化学];
学科分类号
081704 ;
摘要
One hundred and eleven samples of processed fruit juices (apple, grape, pineapple, papaya, guava, banana and mango) and 38 samples of sound fruits (apple, papaya, mango, pear and peach) produced and marketed in Brazil, were analysed for patulin by HPLC. Only one out of 30 samples of apple juice was found positive at 17 mu g/l. Patulin was not detected in the other foodstuffs. It was found in 14 samples of spoiled fruit samples of apple (150-267 mu g/kg), pear (134-245 mu g/kg) and peach (92-174 mu g/kg). Confirmation of the identity of patulin was based on the UV spectrum obtained by the HPLC diode array detector, compared with that of standard patulin, TLC developed by several solvent systems and sprayed with 3-methyl-2-benzothiazolinone hydrazone, and by acetylation with acetic anhydride.
引用
收藏
页码:71 / 74
页数:4
相关论文
共 24 条
[1]  
Becci P J, 1981, J Appl Toxicol, V1, P256, DOI 10.1002/jat.2550010504
[3]  
BURROUGHS LF, 1977, J ASSOC OFF ANA CHEM, V60, P100
[4]   CARCINOGENIC ACTIVITY OF A SERIES OF REACTIVE LACTONES AND RELATED SUBSTANCES [J].
DICKENS, F ;
JONES, HEH .
BRITISH JOURNAL OF CANCER, 1961, 15 (01) :85-&
[5]  
Engel G., 1984, Developments in Food Science, V8, P291
[6]  
FORBITO PR, 1985, J ASSOC OFF ANA CHEM, V68, P950
[7]   Rapid reversed-phase liquid chromatographic determination of patulin in apple juice [J].
Gokmen, V ;
Acar, J .
JOURNAL OF CHROMATOGRAPHY A, 1996, 730 (1-2) :53-58
[8]  
Josefsson E., 1977, Archives de l'Institut Pasteur de Tunis (Tunisia), V54, P261
[9]   COMPARISON OF POTENTIAL PATULIN HAZARD IN HOME-MADE AND COMMERCIAL APPLE PRODUCTS [J].
LINDROTH, S ;
NISKANEN, A .
JOURNAL OF FOOD SCIENCE, 1978, 43 (02) :446-448
[10]  
MACHINSKY M, 1996, ALIMENTARIA, V33, P61