On-line TLC-MS

被引：27

作者：

Prosek, M ^{[1
]}

Milivojevic, L ^{[1
]}

Krizman, M ^{[1
]}

Fir, M ^{[1
]}

机构：

[1] Natl Inst Chem, Ljubljana 1000, Slovenia

来源：

JPC-JOURNAL OF PLANAR CHROMATOGRAPHY-MODERN TLC | 2004年 / 17卷 / 06期

关键词：

TLC; TLC-MS; on-line TLC-MS;

D O I：

10.1556/JPC.17.2004.6.4

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

A new on-line TLC-MS interface, with computer-controlled extraction of substances from selected spots on a TLC or HPTLC plate, has been constructed. The controlled collection of the sample and its programmed injection into the mass spectrometer is the advantage of this type of interface. The interface has been tested and validated with a standard solution of caffeine as test substance. The results were compared with those from a previously established and now routinely used off-line TLC-SPE-APCI-MS extraction procedure.

引用

页码：420 / 423

页数：4

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