Synthesis and characterization of MSe (M = Zn, Cd) nanorods by a new solvothermal method

被引：89

作者：

Wang, WZ ^{[1
]}

Geng, Y

Yan, P

Liu, FY

Xie, Y

Qian, YT

机构：

[1] Univ Sci & Technol China, Dept Chem, Hefei 230026, Anhui, Peoples R China

[2] Univ Sci & Technol China, Struct Res Lab, Hefei 230026, Anhui, Peoples R China

来源：

INORGANIC CHEMISTRY COMMUNICATIONS | 1999年 / 2卷 / 03期

关键词：

nanorod; zinc compounds; cadmium compounds; selenide compounds;

D O I：

10.1016/S1387-7003(99)00015-5

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

The synthesis of one-dimensional nanocrystalline materials is important for scientific research. Here a new solvothermal route to MSe (M = Zn, Cd) nanorods is reported. ZnCl2 (CdCl2), Se and Na were kept in an autoclave at 80-100 degrees C for 4-6 h, and ethylenediamine was chosen as solvent. XRD and TEM were used to characterize the as-prepared MSe (M = Zn,Cd) nanorods. The results showed that diameters of the ZnSe nanorods varied from 40 to 70 nm and the lengths from 1.5 to 3 mu m. The diameters of the CdSe nanorods ranged from 8 to 20 nm and the lengths ranged from 150 to 500 nm. The solvent affected the product quality and morphology. (C) 1999 Elsevier Science S.A. All rights reserved.

引用

页码：83 / 85

页数：3

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