Tetrathiafulvalene (TTF) fused to acenaphthyleno[1,2b][1,4]dithiine:: synthesis and x-ray crystal structure of a new π-electron donor system

被引：6

作者：

Bryce, MR ^{[1
]}

Lay, AK ^{[1
]}

Batsanov, AS ^{[1
]}

Howard, JAK ^{[1
]}

机构：

[1] Univ Durham, Dept Chem, Durham DH1 3LE, England

来源：

TETRAHEDRON LETTERS | 1999年 / 40卷 / 04期

基金：

英国工程与自然科学研究理事会;

关键词：

D O I：

10.1016/S0040-4039(98)02417-4

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

The reaction of transient 1,3-dithiole-2,4,5-trithione 4 with acenaphthylene afforded the Diels-Alder adduct 5, which was dehydrogenated to yield 6; cross-coupling of 6 with 7 gave the tetrathiafulvalene (TTF) derivative 8, which was converted into the di(methylsulfanyl) analogue 10, the solution electrochemistry and X-ray crystal structure of which are reported. (C) 1999 Elsevier Science Ltd. All rights reserved.

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页码：801 / 804

页数：4

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