Identification by HPLC-PAD-MS and quantification by HPLC-PAD of phenylethanoid glycosides of five Phlomis species

被引：67

作者：

Kirmizibekmez, H ^{[1
]}

Montoro, P

Piacente, S

Pizza, C

Dönmez, A

Calis, I

机构：

[1] Hacettepe Univ, Fac Pharm, Dept Pharmacognosy, TR-06100 Ankara, Turkey

[2] Univ Salerno, Dept Pharmaceut Sci, I-84084 Fisciano Salerno, Italy

[3] Hacettepe Univ, Fac Sci, Dept Biol, TR-06532 Ankara, Turkey

来源：

PHYTOCHEMICAL ANALYSIS | 2005年 / 16卷 / 01期

关键词：

HPLC-PAD; HPLC-MS; ESI/MS; phenylethanoid glycosides; Phlomis nissolii; Phlomis leucophractha; Phlomis bruguieri; Phlomis russeliana; Phlomis kurdica;

D O I：

10.1002/pca.802

中图分类号：

Q5 [生物化学];

学科分类号：

071010 [生物化学与分子生物学]; 081704 [应用化学];

摘要：

The qualitative and quantitative determination of phenylethanoid glycosides in methanolic extracts of five species of the genus Phlomis (Lamiaceae) has been investigated using a new reversed-phase HPLC method combined with photodiode-array detection and electrospray/MS analysis. Forsythoside B, verbascoside, samioside, alyssonoside, isoverbascoside, leucosceptosides A and B and martynoside were detected. The quantification of the above constituents was performed using echinacoside as internal standard. Knowledge of the content of phenylethanoid glycosides contributes to the chemotaxonomy of the genus. Copyright (C) 2005 John Wiley Sons, Ltd.

引用

页码：1 / 6

页数：6

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