Studying molecular 3D structure and dynamics by high-resolution solid-state NMR: Application to l-tyrosine-ethylester

被引：33

作者：

Seidel, K

Etzkorn, M

Sonnenberg, L

Griesinger, C

Sebald, A

Baldus, M

机构：

[1] Univ Bayreuth, Bayer Geoinst, D-95440 Bayreuth, Germany

[2] Max Planck Inst Biophys Chem, Dept NMR Based Struct Biol, D-37077 Gottingen, Germany

来源：

JOURNAL OF PHYSICAL CHEMISTRY A | 2005年 / 109卷 / 11期

关键词：

D O I：

10.1021/jp045605m

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

A unified approach to the study of 3D conformation and molecular dynamics using magic-angle-spinning solid-state NMR is demonstrated on a uniformly C-13-labeled sample of 1-tyrosine-ethylester.

引用

页码：2436 / 2442

页数：7

共 54 条

[1] NUCLEAR MAGNETIC RESONANCE SPECTRA FROM A CRYSTAL ROTATED AT HIGH SPEED [J].

ANDREW, ER ;

BRADBURY, A ;

EADES, RG .

NATURE, 1958, 182 (4650) :1659-1659

[2] Broadband polarization transfer under magic-angle spinning: Application to total through-space-correlation NMR spectroscopy [J].

Baldus, M ;

Meier, BH .

JOURNAL OF MAGNETIC RESONANCE, 1997, 128 (02) :172-193

[3] Correlation experiments for assignment and structure elucidation of immobilized polypeptides under magic angle spinning [J].

Baldus, M .

PROGRESS IN NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY, 2002, 41 (1-2) :1-47

[4] HETERONUCLEAR DECOUPLING IN ROTATING SOLIDS [J].

BENNETT, AE ;

RIENSTRA, CM ;

AUGER, M ;

LAKSHMI, KV ;

GRIFFIN, RG .

JOURNAL OF CHEMICAL PHYSICS, 1995, 103 (16) :6951-6958

[5] FREQUENCY-SWITCHED PULSE SEQUENCES - HOMONUCLEAR DECOUPLING AND DILUTE SPIN NMR IN SOLIDS [J].

BIELECKI, A ;

KOLBERT, AC ;

LEVITT, MH .

CHEMICAL PHYSICS LETTERS, 1989, 155 (4-5) :341-346

[6] Advanced solid-state NMR methods for the elucidation of structure and dynamics of molecular, macromolecular, and supramolecular systems [J].

Brown, SP ;

Spiess, HW .

CHEMICAL REVIEWS, 2001, 101 (12) :4125-4155

[7]

Brunger AT, 1998, ACTA CRYSTALLOGR D, V54, P905, DOI 10.1107/s0907444998003254

[8] HETERONUCLEAR CORRELATION SPECTROSCOPY IN ROTATING SOLIDS [J].

CARAVATTI, P ;

BRAUNSCHWEILER, L ;

ERNST, RR .

CHEMICAL PHYSICS LETTERS, 1983, 100 (04) :305-310

[9] Structure of a protein determined by solid-state magic-angle-spinning NMR spectroscopy [J].

Castellani, F ;

van Rossum, B ;

Diehl, A ;

Schubert, M ;

Rehbein, K ;

Oschkinat, H .

NATURE, 2002, 420 (6911) :98-102

[10] Rotational resonance tickling: Accurate internuclear distance measurement in solids [J].

Costa, PR ;

Sun, BQ ;

Griffin, RG .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1997, 119 (44) :10821-10830

← 1 2 3 4 5 6 →