Preparation and characterization of CuInS2 nanorods and nanotubes from an elemental solvothermal reaction

被引：43

作者：

Jiang, Y

Qu, Y

Yuan, SW

Xie, B

Zhang, SY

Qian, YT ^{[1
]}

机构：

[1] Univ Sci & Technol China, Dept Chem, Hefei 230026, Anhui, Peoples R China

[2] Univ Sci & Technol China, Struct Res Lab, Hefei 230026, Anhui, Peoples R China

来源：

JOURNAL OF MATERIALS RESEARCH | 2001年 / 16卷 / 10期

基金：

中国国家自然科学基金;

关键词：

D O I：

10.1557/JMR.2001.0386

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

A simple and convenient solvothermal reaction has been developed to produce CuInS2 nanorods and nanotubes from the elements in ethylenediamine at 280 degreesC. The products were characterized by x-ray diffraction, transmission electron microscopy, high-resolution transmission electron microscopy, scanning electron microscopy, and x-ray photoelectron spectroscopy. Analysis shows that the coordinating ability of ethylenediamine and the existence of liquid In may play important roles in the growth of one-dimension nanocrystallites and the electron-transfer reaction. In addition, spherical CuInS2 micrometer particles were obtained at 350 degreesC.

引用

页码：2805 / 2809

页数：5

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