Routine gas chromatographic determination of dialkylphosphate metabolites in the urine of workers occupationally exposed to organophosphorus insecticides

被引：28

作者：

Oglobline, AN ^{[1
]}

O'Donnell, GE

Geyer, R

Holder, GM

Tattam, B

机构：

[1] WorkCover New S Wales, Lab Serv, Thornleigh, NSW 2120, Australia

[2] Univ Sydney, Fac Pharm, Sydney, NSW 2006, Australia

来源：

JOURNAL OF ANALYTICAL TOXICOLOGY | 2001年 / 25卷 / 03期

关键词：

D O I：

10.1093/jat/25.3.153

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

A routine gas chromatographic (GC) method is described for the analysis of dialkylphosphate metabolites in the urine of workers occupationally exposed to organophosphorus insecticides. The procedure involves derivatizing a freeze-dried urine sample with pentafluorobenzyl bromide and then determining the metabolites using dual capillary column GC with flame photometric detection.

引用

页码：153 / 157

页数：5

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