Sonochemical synthesis of a new nano-plate lead(II) coordination polymer constructed of maleic acid

被引：26

作者：

Aboutorabi, Leila ^{[2
]}

Morsali, Ali ^{[1
]}

机构：

[1] Tarbiat Modares Univ, Fac Sci, Dept Chem, Tehran, Iran

[2] Payame Noor Univ, Dept Chem, Abhar, Zanjan, Iran

来源：

INORGANICA CHIMICA ACTA | 2010年 / 363卷 / 11期

关键词：

Nano-plate; Lead(II) oxide; Maleic acid; Crystal structure;

D O I：

10.1016/j.ica.2010.04.024

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

A new nano-sized lead(II) coordination polymer of maleic acid (H(2)Mal), [Pb(mu(7)-Mal)](n) (1), has been synthesized by sonochemical method and characterized by scanning electron microscopy, X-ray powder diffraction, elemental analyses and IR spectroscopy. The compound 1 was structurally characterized by single-crystal X-ray diffraction. Thermal stability of nano and bulk samples of compound 1 were studied and compared with each other. After calcination of nano-sized compound 1 at 600 degrees C, pure phase microsized lead(II) oxide has been produced. (C) 2010 Elsevier B.V. All rights reserved.

引用

页码：2506 / 2511

页数：6

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