Study on the feasibility of coupling large-volume injection to fast gas chromatography with mass spectrometric detection for analysis of organochlorine pesticides

被引：18

作者：

Korenková, E

Matisová, E

Slobodník, J

机构：

[1] Inst Environm, Kosice 97241, Slovakia

[2] Slovak Univ Technol Bratislava, Dept Analyt Chem, Fac Chem & Food Technol, Bratislava 81237, Slovakia

来源：

JOURNAL OF SEPARATION SCIENCE | 2003年 / 26卷 / 12-13期

关键词：

programmable temperature vaporisation injector; fast GC; organochlorine compounds; pesticide residues;

D O I：

10.1002/jssc.200301269

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

A combined use of programmable temperature vaporisation injector, fast oven temperature ramp, 0.1 mm ID analytical column and hydrogen carrier gas enabled injection of up to 20 muL of extract containing 15 organochlorine pesticides and separation of all analytes in less than 8 minutes.

引用

页码：1193 / 1197

页数：5

共 13 条

[1] Determination of pesticides in environmental waters by solid-phase extraction and gas chromatography with electron-capture and mass spectrometry detection [J].