The certification of SRM 1546 - Meat Homogenate, a new reference material for nutrients in a high protein, high fat matrix

被引:14
作者
Welch, MJ [1 ]
Colbert, JC [1 ]
Gill, LM [1 ]
Phinney, CS [1 ]
Sharpless, KE [1 ]
Sniegoski, LT [1 ]
Wood, LJ [1 ]
机构
[1] NIST, Div Analyt Chem, Chem Sci & Technol Lab, US Dept Commerce, Gaithersburg, MD 20899 USA
来源
FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY | 2001年 / 370卷 / 01期
关键词
D O I
10.1007/s002160100705
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
In response to reference material needs expressed by the food industry and government regulators, the National Institute of Standards and Technology (NIST) has developed a new Standard Reference Material (SRM) consisting of a canned meat product with certified and reference values for a large number of constituents. SRM 1546 Meat Homogenate consists of a mixture of finely ground pork and chicken prepared and canned by a commercial process. NIST determined the concentration levels of cholesterol, sodium, calcium, iron, and seven fatty acids in this SRM using well defined methods and procedures. These analytes as well as 34 other constituents or properties were determined in an interlaboratory comparison exercise involving 21 laboratories, most of which are associated with the National Food Processors Association (NFPA) Food Industry Analytical Chemists Subcommittee (FIACS). From statistical analysis of the data, NIST assigned certified concentrations for the eleven analytes measured at NIST and reference concentrations for the proximates, six additional fatty acids, seven minerals, and seven water-soluble vitamins. Information values without uncertainties are provided for the concentrations of six additional constituents for which the uncertainties could not adequately be assessed. SRM 1546 will provide Laboratories with a means to evaluate the accuracy of the methods they use to assign nutrient levels to processed meats and similar products.
引用
收藏
页码:42 / 47
页数:6
相关论文
共 13 条
[1]  
[Anonymous], 2000, NIST SPECIAL PUBLICA
[2]  
*AOAC INT, 1997, OFF METH AN S, pB18
[3]  
*AOAC INT, 1980, 43235 AOAC INT
[4]  
AOAC International, 1980, OFF METH AN, V13th
[5]   DETERMINATION OF SERUM-CHOLESTEROL BY A MODIFICATION OF THE ISOTOPE-DILUTION MASS-SPECTROMETRIC DEFINITIVE METHOD [J].
ELLERBE, P ;
MEISELMAN, S ;
SNIEGOSKI, LT ;
WELCH, MJ ;
WHITE, E .
ANALYTICAL CHEMISTRY, 1989, 61 (15) :1718-1723
[6]   DETERMINATION OF TOTAL CHOLESTEROL IN COCONUT OIL - A NEW NIST CHOLESTEROL STANDARD REFERENCE MATERIAL [J].
ELLERBE, PM ;
SNIEGOSKI, LT ;
WELCH, MJ ;
WHITE, E .
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1989, 37 (04) :954-957
[7]  
International Organization for Standardization, 1993, GUID EXPR UNC MEAS
[8]   COMBINING DATA FROM INDEPENDENT CHEMICAL-ANALYSIS METHODS [J].
SCHILLER, SB ;
EBERHARDT, KR .
SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY, 1991, 46 (12) :1607-1613
[9]  
Sharpless KE, 1999, J AOAC INT, V82, P288
[10]  
Sharpless KE, 1997, J AOAC INT, V80, P611