endo-(1′R,′R,5′S,7′R,9′S)-2-(9′-Benzyloxy-2′-phenyl-3′,6′-dioxabicyclo[3.2.2]nonan-7′-yl)-7-bromo-5,8-dimethoxynaphthalen-1-yl acetate

被引：2

作者：

Brenstrum, TJ ^{[1
]}

Brimble, MA ^{[1
]}

Turner, P ^{[1
]}

机构：

[1] Univ Sydney, Sch Chem, Camperdown, NSW 2006, Australia

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2001年 / 57卷

关键词：

D O I：

10.1107/S1600536800018092

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The title compound, (1), is the product of a model synthesis of an analogue of the antibiotic medermycin, and is thought to be the result of an unusual 1,6-hydride shift.

引用

页码：O28 / O29

页数：2

共 13 条

[1] COMPLETION AND REFINEMENT OF CRYSTAL-STRUCTURES WITH SIR92 [J].

ALTOMARE, A ;

CASCARANO, G ;

GIACOVAZZO, C ;

GUAGLIARDI, A .

JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1993, 26 (pt 3) :343-350

[2] LEAST-SQUARES ABSOLUTE-STRUCTURE REFINEMENT - PRACTICAL EXPERIENCE AND ANCILLARY CALCULATIONS [J].

BERNARDINELLI, G ;

FLACK, HD .

ACTA CRYSTALLOGRAPHICA SECTION A, 1985, 41 (SEP) :500-511

[3] Synthesis of naphthyl C-glycosides of rearranged tri-O-benzyl-2-deoxy-D-glucose [J].

Brimble, MA ;

Brenstrum, TJ .

TETRAHEDRON LETTERS, 2000, 41 (07) :1107-1110

[4] Acetyl perchlorate mediated rearrangement of tri-O-benzyl-D-glucal. Evidence for a 1,6-hydride shift [J].

Byerley, ALJ ;

Kenwright, AM ;

Lehmann, CW ;

MacBride, JAH ;

Steel, PG .

JOURNAL OF ORGANIC CHEMISTRY, 1998, 63 (01) :193-194

[5] ON ENANTIOMORPH-POLARITY ESTIMATION [J].

FLACK, HD .

ACTA CRYSTALLOGRAPHICA SECTION A, 1983, 39 (NOV) :876-881

[6]

HALL SR, 1999, XTAL3 6 SYSTEM

[7]

Johnson C. K., 1976, ORNL5138

[8]

*MOL STRUCT CORP, 1995, MSC AFC DIFFR CONTR

[9]

*MOL STRUCT CORP, 1992, TEXSAN UNIX VERS 1 8

[10]

*MOL STRUCT CORP, 1997, TEXSAN WIND

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