Microwave-assisted synthesis of metal sulfides in ethylene glycol

被引：110

作者：

Chen, D

Tang, KB ^{[1
]}

Shen, GZ

Sheng, J

Fang, Z

Liu, XM

Zheng, HG

Qian, YT

机构：

[1] Univ Sci & Technol China, Dept Chem, Hefei 230026, Peoples R China

[2] Univ Sci & Technol China, Struct Res Lab, Hefei 230026, Peoples R China

来源：

MATERIALS CHEMISTRY AND PHYSICS | 2003年 / 82卷 / 01期

基金：

中国国家自然科学基金;

关键词：

chalcogenides; chemical synthesis; electron microscopy;

D O I：

10.1016/S0254-0584(03)00206-2

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

Metal sulfides MS (M = Cd, Zn, Co, Pb, CU), M2S3 (M = Bi, Sb), M2S (M = Ag) were successfully synthesized through a one-step reaction between metal salts and thiourea in ethylene glycol (EG) under the microwave irradiation. The products were characterized by powder X-ray diffraction (XRD), X-ray photoelectron spectroscope (XPS), transmission electron microscope (TEM) and electron diffraction (ED). (C) 2003 Elsevier B.V. All rights reserved.

引用

页码：206 / 209

页数：4

共 31 条

[1] [Anonymous], CERAMIC POWDER SCI
[2] Bykov Y. V., 1997, CERAM T, V80, P321
[3] COUSTAL R, 1958, J CHIM PHYS PCB, V38, P277
[4] DUTAULT F, 1979, B SOC CHIM FR, V5, P145
[5] Polyol mediated synthesis of nanoscale MS particles (M = Zn, Cd, Hg)
Feldmann, C
Metzmacher, C
[J]. JOURNAL OF MATERIALS CHEMISTRY, 2001, 11 (10) : 2603 - 2606
[6] Convenient, low-energy synthesis of metal sulfides and selenides; PbE, Ag(2)E, ZnE, CdE (E=S, Se)
Henshaw, G
Parkin, IP
Shaw, G
[J]. CHEMICAL COMMUNICATIONS, 1996, (10) : 1095 - 1096
[7] KANATZIDIS MG, 1995, PROG INORG CHEM, V43, P151, DOI 10.1002/9780470166444.ch2
[8] MOLTEN ALKALI-METAL POLYCHALCOGENIDES AS REAGENTS AND SOLVENTS FOR THE SYNTHESIS OF NEW CHALCOGENIDE MATERIALS
KANATZIDIS, MG
[J]. CHEMISTRY OF MATERIALS, 1990, 2 (04) : 353 - 363
[9] KERM KV, 1980, P TALLINN TU, P101
[10] Sonochemical and microwave-assisted preparations of PbTe and PbSe. A comparative study
Kerner, R
Palchik, O
Gedanken, A
[J]. CHEMISTRY OF MATERIALS, 2001, 13 (04) : 1413 - 1419

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