Synthesis and X-ray crystal structure of a novel long chain acyclic phosphazene, N,N′-{dimethyl-bis(diphenylphosphiniminophosphorane)} ethylenediamine {(PhO)2P(O)N=PN(CH3)CH2}2, obtained via a Staudinger reaction

被引：30

作者：

Balakrishna, MS ^{[1
]}

Abhyankar, RM ^{[1
]}

Walawalker, MG ^{[1
]}

机构：

[1] Indian Inst Technol, Dept Chem, Bombay 400076, Maharashtra, India

来源：

TETRAHEDRON LETTERS | 2001年 / 42卷 / 14期

关键词：

phosphazene; phosphinimines; Staudinger reaction; X-ray structure;

D O I：

10.1016/S0040-4039(01)00236-2

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

The title compound was synthesized by the reaction of N,N'-dimethyl-N,N'-bis(diphenylphosphino)ethylenediamine with phosphoryl azide and characterized by mass spectrometry, microanalysis, and P-31 and (1) NMR spectroscopy and the structure was confirmed by single crystal X-ray studies. (C) 2001 Elsevier Science Ltd. All rights reserved.

引用

页码：2733 / 2734

页数：2

共 10 条

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