Coherent small-angle scattering on a bending-magnet beamline at the ESRF

被引:18
作者
Livet, F
Bley, F
Létoublon, A
Simon, JP
Bérar, JF
机构
[1] Ecole Natl Super Electrochim & Electrom Gren, Thermodynam & Physicochim Met Lab, CNRS,UMR, INPG,UJF 5614, F-38402 St Martin Dheres, France
[2] CNRS, Cristallog Lab, F-38402 Grenoble, France
关键词
coherent X-rays; small-angle scattering; speckle;
D O I
10.1107/S0909049598007353
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
A coherent X-ray beam is obtained from the D2AM bending-magnet beamline (BM2) of the European Synchrotron Radiation Facility. As this line has permanent convergent optics, monochromated by an Si(111) double monochromator, coherence conditions are satisfied by selecting a part of the beam close to the focal point. Low intensity (10(6) X-rays s(-1)) is partially compensated by a high degree of coherence and by the use of a high-resolution direct-illumination CCD area detector. The stability of the small-angle set-up makes quantitative analysis possible. The calculated and measured degrees of coherence are compared. The distributions of speckle intensities are explained by a beam composed of two-thirds coherent and one-third incoherent parts. This incoherent component is caused by Kapton windows, which will be removed in future experiments.
引用
收藏
页码:1337 / 1345
页数:9
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