Crystal structure and spectroscopic data of fac-tricarbonylbromo(3,3'-trimethylene-2,2'-bi-1,8-naphthyridine)rhenium(I), Re(CO)(3)Br(C19H14N4)

被引:18
作者
Moya, SA
Schmidt, R
Pastene, R
Sartori, R
Muller, U
Frenzen, G
机构
[1] UNIV SANTIAGO CHILE,FAC QUIM & BIOL,DEPT QUIM APLICADA,SANTIAGO,CHILE
[2] UNIV GESAMTHSCH KASSEL,FACHBEREICH BIOL CHEM,D-34109 KASSEL,GERMANY
关键词
D O I
10.1021/om960107o
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
The title compound 1 was obtained from Re(CO)(5)Br and the binaphthyridine in heptane. Its X-ray crystal structure determination shows a molecular structure with the two nitrogen atoms in positions 1 and 1' acting as a bidentate chelate ligand to the Re atom. H-1 NMR, UV-vis, and IR spectroscopic data are reported and assigned.
引用
收藏
页码:3463 / 3465
页数:3
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