Preparation of cellulose oligomers from cellulose triacetate (standard procedure)

被引：6

作者：

Arndt, P ^{[1
]}

Gerdes, R ^{[1
]}

Huschens, S ^{[1
]}

Pyplo-Schnieders, J ^{[1
]}

Redlich, H ^{[1
]}

机构：

[1] Univ Munster, Inst Organ Chem, D-48149 Munster, Germany

来源：

CELLULOSE | 2005年 / 12卷 / 03期

关键词：

cellulose; cellulose oligomers; pivaloylysis;

D O I：

10.1007/s10570-004-3387-6

中图分类号：

TB3 [工程材料学]; TS [轻工业、手工业、生活服务业];

学科分类号：

0805 ; 080502 ; 0822 ;

摘要：

This communication reports the detailed procedure for the cleavage of cellulose triacetate (30 g scale) with pivalic anhydride and boron trifluoride etherate in dichloromethane (pivaloylysis). With this mild and efficient method the cellulose oligomers up to the octasaccharide can be obtained in gram scale. Full characteristic data of this compounds are given.

引用

页码：317 / 326

页数：10

共 8 条

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