Degradation of historical paper:: nondestructive analysis by the NMR-MOUSE

被引:81
作者
Blümich, B
Anferova, S
Sharma, S
Segre, AL
Federici, C
机构
[1] Rhein Westfal TH Aachen, Inst Tech & Makromol Chem, D-52056 Aachen, Germany
[2] Kaliningrad State Univ, Kaliningrad 236041, Russia
[3] CNR, Inst Chem Methodol, I-00016 Monterotondo, Rome, Italy
[4] Inst Cent Patol Libro, I-00184 Rome, Italy
关键词
NMR-MOUSE; unilateral NMR; historical paper; degradation; cultural heritage;
D O I
10.1016/S1090-7807(03)00034-X
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
The NMR-MOUSE is a mobile sensor for single-sided NMR inspection of organic materials which takes advantage of the principles of magnetic resonance and inside-out-NMR. Historical books dating from the 17th century were measured at different points by positioning the NMR-MOUSE on the paper. Different degrees of paper degradation can be discriminated from the regularized inverse Laplace transform of the envelope of the acquired echo signals. For the first time the degradation of historical paper was characterized entirely nondestructively by NMR. As a contribution to current preservation efforts, NMR shows great promise for future use in damage assessment of historical documents. (C) 2003 Elsevier Science (USA). All rights reserved.
引用
收藏
页码:204 / 209
页数:6
相关论文
共 33 条
[1]   Construction of a NMR-MOUSE with short dead time [J].
Anferova, S ;
Anferov, V ;
Adams, M ;
Blümler, P ;
Routley, N ;
Hailu, K ;
Kupferschläger, K ;
Mallett, MJD ;
Schroeder, G ;
Sharma, S ;
Blümich, B .
CONCEPTS IN MAGNETIC RESONANCE, 2002, 15 (01) :15-25
[2]   Nuclear magnetic resonance in inhomogeneous magnetic fields [J].
Balibanu, F ;
Hailu, K ;
Eymael, R ;
Demco, DE ;
Blümich, B .
JOURNAL OF MAGNETIC RESONANCE, 2000, 145 (02) :246-258
[3]  
Bl?mich B., 2000, NMR IMAGING MAT
[4]   The NMR-mouse:: Construction, excitation, and applications [J].
Blümich, B ;
Blümler, P ;
Eidmann, G ;
Guthausen, A ;
Haken, R ;
Schmitz, U ;
Saito, K ;
Zimmer, G .
MAGNETIC RESONANCE IMAGING, 1998, 16 (5-6) :479-484
[5]   Uniform-penalty inversion of multiexponential decay data [J].
Borgia, GC ;
Brown, RJS ;
Fantazzini, P .
JOURNAL OF MAGNETIC RESONANCE, 1998, 132 (01) :65-77
[6]   Examples of uniform-penalty inversion of multiexponential relaxation data [J].
Borgia, GC ;
Brown, RJS ;
Fantazzini, P .
MAGNETIC RESONANCE IMAGING, 1998, 16 (5-6) :549-552
[7]  
CALLAGHAN PT, 1991, PRINCIPALS NUCL MAGN
[8]  
Capitani D, 1996, TAPPI J, V79, P113
[9]   Early detection of enzymatic attack on paper by NMR relaxometry, EPR spectroscopy and X-Ray powder spectra [J].
Capitani, D ;
Emanuele, MC ;
Segre, A ;
Fanelli, C ;
Fabbri, AA ;
Attanasio, D ;
Focher, B ;
Capretti, G .
NORDIC PULP & PAPER RESEARCH JOURNAL, 1998, 13 (02) :95-100
[10]   NMR study of water-filled pores in one of the most widely used polymeric material: The paper [J].
Capitani, D ;
Proietti, N ;
Ziarelli, F ;
Segre, AL .
MACROMOLECULES, 2002, 35 (14) :5536-5543