Isolation and characterization of all eight bisadducts of fulleropyrrolidine derivatives

被引:119
作者
Kordatos, K
Bosi, S
Da Ros, T
Zambon, A
Lucchini, V
Prato, M
机构
[1] Univ Trieste, Dipartimento Sci Farmaceut, I-34127 Trieste, Italy
[2] Univ Venice, Dipartimento Sci Ambientali, I-30133 Venice, Italy
关键词
D O I
10.1021/jo001708z
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
We report the isolation and characterization of bisadducts of fulleropyrrolidine derivatives. The compounds were characterized by means of a variety of spectroscopic techniques, including ES-MS, UV-vis, H-1 NMR, and C-13 NMR. The whole series of bisadducts was separated for the first time in the case of the bispyrrolidines, and the determination of their structure was obtained by NMR spectroscopy with the help of HMQC and HMBC techniques.
引用
收藏
页码:2802 / 2808
页数:7
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