Formation of γ-alumina nanorods in presence of alanine

被引:17
作者
Dabbagh, Hossein A. [1 ]
Rasti, Elham [1 ]
Yalfani, Mohammad S. [2 ]
Medina, Francesc [2 ]
机构
[1] Isfahan Univ Technol, Dept Chem, Catalysis Res Lab, Esfahan 8415483111, Iran
[2] Univ Rovira & Virgili, Dept Engn Quim, Tarragona 43007, Spain
关键词
Oxides; Nanostructure; Sol-gel chemistry; X-ray diffraction; Electron microscopy; SURFACTANT-ASSISTED SYNTHESIS; MESOPOROUS METAL-OXIDES; IN-SITU SYNTHESIS; BOEHMITE NANOFIBERS; MOLECULAR-SIEVES; GEL SYNTHESIS; ROUTE; NANOPARTICLES; ADSORPTION; SILICA;
D O I
10.1016/j.materresbull.2010.10.011
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Boehmite and alumina nanostructures were prepared using a simple green sol-gel process in the presence of alanine in water medium at room temperature. The uncalcined (dried at 200 degrees C) and the calcined materials (at 500, 600 and 700 degrees C for 4 h) were characterized using XRD, TEM, SEM, N-2 physisorption and TGA. Nanorod aluminas with a possible hexagonal symmetry, high surface area and relatively narrow pore size distribution were obtained. The surface area was enhanced and crystallization was retarded as the alanine content increased. The morphologies of the nanoparticles and nanorods were revealed by a transmission electron microscope (TEM). (C) 2010 Elsevier Ltd. All rights reserved.
引用
收藏
页码:271 / 277
页数:7
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