Zinc promoted convenient and general synthesis of thiol esters

被引：48

作者：

Meshram, HM ^{[1
]}

Reddy, GS ^{[1
]}

Bindu, KH ^{[1
]}

Yadav, JS ^{[1
]}

机构：

[1] Indian Inst Chem Technol, Hyderabad 500007, Andhra Pradesh, India

来源：

SYNLETT | 1998年 / 08期

关键词：

zinc; thiol ester; acid chloride; nucleophilic displacement; electrophilic character;

D O I：

10.1055/s-1998-1797

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Synthesis of thiol esters from acyl chlorides and thiols in the presence of activated zinc is described. The recovery of zinc and its reuse makes the procedure more economic.

引用

页码：877 / +

页数：3

共 36 条

[1]

BACHILLER FS, 1976, J CHEM SOC CHEM COMM, P719

[2] SYNTHESIS OF MACROCYCLIC LACTONES - APPROACHES TO COMPLEX MACROLIDE ANTIBIOTICS [J].

BACK, TG .

TETRAHEDRON, 1977, 33 (23) :3041-3059

[3] Cadmium promoted allylation of acid chlorides: Synthesis of beta,gamma-unsaturated ketones [J].

Baruah, B ;

Boruah, A ;

Prajapati, D ;

Sandhu, JS .

TETRAHEDRON LETTERS, 1996, 37 (50) :9087-9088

[4] REDUCTION OF THIOL ESTERS BY LITHIUM ALUMINUM HYDRIDE-ALUMINUM CHLORIDE [J].

BUBLITZ, DE .

JOURNAL OF ORGANIC CHEMISTRY, 1967, 32 (05) :1630-&

[5] ORGANOMANGANESE(II) REAGENTS .19. ACYLATION OF ORGANOMANGANESE CHLORIDES BY CARBOXYLIC-ACID CHLORIDES IN THF - A CLEAR IMPROVEMENT IN THE FIELD OF THE PREPARATION OF KETONES FROM ORGANOMANGANESE COMPOUNDS [J].

CAHIEZ, G ;

LABOUE, B .

TETRAHEDRON LETTERS, 1989, 30 (52) :7369-7372

[6] ALKOXY- THIO- AND AMINO-DERIVATIVES OF METHYLZINC [J].

COATES, GE ;

RIDLEY, D .

JOURNAL OF THE CHEMICAL SOCIETY, 1965, (MAR) :1870-&

[7]

COHEN T, 1978, TETRAHEDRON LETT, V45, P4319

[8]

COREY EJ, 1977, TETRAHEDRON LETT, V18, P3919

[9] PENEMS, A NEW CLASS OF BETA-LACTAM ANTIBIOTICS - 6-ACYLAMINOPENEM-3-CARBOXYLIC ACIDS [J].

ERNEST, I ;

GOSTELI, J ;

GREENGRASS, CW ;

HOLICK, W ;

JACKMAN, DE ;

PFAENDLER, HR ;

WOODWARD, RB .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1978, 100 (26) :8214-8222

[10]

FURSTNER A, 1989, SYNTHESIS-STUTTGART, P571

← 1 2 3 4 →