Hydrothermal synthesis of MoS2 and its pressure-related crystallization

被引:152
作者
Peng, YY [1 ]
Meng, ZY
Zhong, C
Lu, J
Yu, WC
Yang, ZP
Qian, YT
机构
[1] Univ Sci & Technol China, Dept Chem, Hefei 230026, Anhui, Peoples R China
[2] Univ Sci & Technol China, Struct Res Lab, Hefei 230026, Anhui, Peoples R China
关键词
MoS2; single-layer; pressure-related; hydrothermal;
D O I
10.1006/jssc.2001.9146
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
Crystalline, poorly crystalline, and single-layer MoS2 were synthesized using a hydrothermal method at low temperature (170-200 degreesC) through changing pressure and time. XPS, XRD, and TEM were used to study the products. It was found that the stacking of the single layers was closely related to the pressure in the autoclave, A model was presented to explain this phenomenon. (C) 2001 Academic Press.
引用
收藏
页码:170 / 173
页数:4
相关论文
共 22 条
[1]   Surfactant-assisted synthesis of highly dispersed molybdenum sulfide [J].
Afanasiev, P ;
Xia, GF ;
Berhault, G ;
Jouguet, B ;
Lacroix, M .
CHEMISTRY OF MATERIALS, 1999, 11 (11) :3216-3219
[2]   PREPARATION AND CHARACTERIZATION OF A NEW CRYSTALLINE FORM OF MOLYBDENUM DISULFIDE [J].
BELL, RE ;
HERFERT, RE .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1957, 79 (13) :3351-3354
[3]   RAPID SOLID-STATE SYNTHESIS OF MATERIALS FROM MOLYBDENUM-DISULFIDE TO REFRACTORIES [J].
BONNEAU, PR ;
JARVIS, RF ;
KANER, RB .
NATURE, 1991, 349 (6309) :510-512
[4]   LOW-TEMPERATURE CHEMICAL PREPARATION OF SEMICONDUCTING TRANSITION-METAL CHALCOGENIDE FILMS FOR ENERGY-CONVERSION AND STORAGE, LUBRICATION AND SURFACE PROTECTION [J].
CHATZITHEODOROU, G ;
FIECHTER, S ;
KUNST, M ;
LUCK, J ;
TRIBUTSCH, H .
MATERIALS RESEARCH BULLETIN, 1988, 23 (09) :1261-1271
[5]   LOW-TEMPERATURE SOLUTION PREPARATION OF GROUP 4B, 5B, AND 6B TRANSITION-METAL DICHALCOGENIDES [J].
CHIANELLI, RR ;
DINES, MB .
INORGANIC CHEMISTRY, 1978, 17 (10) :2758-2762
[6]   MOLYBDENUM-DISULFIDE IN THE POORLY CRYSTALLINE RAG STRUCTURE [J].
CHIANELLI, RR ;
PRESTRIDGE, EB ;
PECORARO, TA ;
DENEUFVILLE, JP .
SCIENCE, 1979, 203 (4385) :1105-1107
[7]   FUNDAMENTAL-STUDIES OF TRANSITION-METAL SULFIDE HYDRODESULFURIZATION CATALYSTS [J].
CHIANELLI, RR .
CATALYSIS REVIEWS-SCIENCE AND ENGINEERING, 1984, 26 (3-4) :361-393
[8]   SURFACE SPECTROSCOPIC CHARACTERIZATION OF COBALT MOLYBDENUM ALUMINA CATALYSTS [J].
CHIN, RL ;
HERCULES, DM .
JOURNAL OF PHYSICAL CHEMISTRY, 1982, 86 (16) :3079-3089
[9]  
Clauss F. J., 1972, SOLID LUBRICANTS SEL
[10]   THERMAL-DECOMPOSITION OF (NH4)2[MO3S(S2)6] . NH2O [J].
DIEMANN, E ;
MULLER, A ;
AYMONINO, PJ .
ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 1981, 479 (08) :191-198