A facile cleavage of allyl ethers on solid phase

被引:20
作者
Opatz, T [1 ]
Kunz, H [1 ]
机构
[1] Univ Mainz, Inst Organ Chem, D-55128 Mainz, Germany
关键词
solid-phase synthesis; allyl ethers; protecting groups; palladium;
D O I
10.1016/S0040-4039(00)01835-9
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
A simple and efficient protocol for the cleavage of allyl ethers on solid phase using a palladium(0)catalyzed allyl transfer reaction is reported. (C) 2000 Elsevier Science Ltd. All rights reserved.
引用
收藏
页码:10185 / 10188
页数:4
相关论文
共 20 条
[1]   ORGANO HALIDE ADDITION TO PD2(PH2PCH2PPH2)3 - PREPARATION OF NOVEL METHYLENE-BRIDGED AND PHENYLENE-BRIDGED COMPLEXES BY 2-CENTER, 3-FRAGMENT OXIDATIVE ADDITION [J].
BALCH, AL ;
HUNT, CT ;
LEE, CL ;
OLMSTEAD, MM ;
FARR, JP .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1981, 103 (13) :3764-3772
[2]  
Balkenhohl F, 1996, ANGEW CHEM INT EDIT, V35, P2289
[3]  
BUNIN BA, 1998, COMBINATORIAL INDEX
[4]   Moenomycin A:: The role of the methyl group in the moenuronamide unit and a general discussion of structure-activity relationships [J].
El-Abadla, N ;
Lampilas, M ;
Hennig, L ;
Findeisen, M ;
Welzel, P ;
Müller, D ;
Markus, A ;
van Heijenoort, J .
TETRAHEDRON, 1999, 55 (03) :699-722
[5]   Organic chemistry on solid supports [J].
Fruchtel, JS ;
Jung, G .
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION IN ENGLISH, 1996, 35 (01) :17-42
[6]   Allylic protecting groups and their use in a complex environment -: Part II:: Allylic protecting groups and their removal through catalytic palladium π-allyl methodology [J].
Guibé, F .
TETRAHEDRON, 1998, 54 (13) :2967-3042
[7]   Allylic protecting groups and their use in a complete environment .1. Allylic protection of alcohols [J].
Guibe, F .
TETRAHEDRON, 1997, 53 (40) :13509-13556
[8]   Deprotection of allyl groups with sulfinic acids and palladium catalyst [J].
Honda, M ;
Morita, H ;
Nagakura, I .
JOURNAL OF ORGANIC CHEMISTRY, 1997, 62 (25) :8932-8936
[9]  
Jung G., 1999, COMBINATORIAL CHEM
[10]   Combinatorial solid-phase synthesis using D-Galactose as a chiral five-dimension-diversity scaffold [J].
Kallus, C ;
Opatz, T ;
Wunberg, T ;
Schmidt, W ;
Henke, S ;
Kunz, H .
TETRAHEDRON LETTERS, 1999, 40 (44) :7783-7786