Simulation of the sintering behavior of a ceramic green body using advanced thermokinetic analysis

被引:35
作者
Opfermann, J [1 ]
Blumm, J [1 ]
Emmerich, WD [1 ]
机构
[1] NETZSCH Geratebau GMBH, D-95100 Selb, Bavaria, Germany
关键词
alumina; sintering; kinetics; rate controlled thermal analysis; simulations;
D O I
10.1016/S0040-6031(98)00345-1
中图分类号
O414.1 [热力学];
学科分类号
摘要
The sintering behavior of an alumina green body was measured at three different heating rates using a high-temperature pushrod dilatometer. The measurement results were evaluated with a complex thermokinetic analysis program. Using the calculated kinetic parameters, predictions were made for the behavior under rate controlled sintering conditions. The resulting temperature profiles were compared with the results of actual rate controlled sintering measurements. Good agreement was found between the experimental data and the thermokinetic prediction. (C) 1998 Elsevier Science B.V.
引用
收藏
页码:213 / 220
页数:8
相关论文
共 16 条
[1]  
FRIEDMAN HL, 1965, J POLYM SCI C, V6, P175
[2]   STUDY OF SPECIAL CERAMICS WITH A DILATOMETER IN THE TEMPERATURE-RANGE 25-DEGREEC-C-2000-DEGREES-C [J].
KAISERSBERGER, E ;
KELLY, J .
INTERNATIONAL JOURNAL OF THERMOPHYSICS, 1989, 10 (02) :505-512
[3]  
Kaisersberger E, 1992, LABORPRAXIS, V4, P360
[4]   PREDICTION OF THE THERMAL RESPONSE OF HAZARDOUS MATERIALS DURING STORAGE USING AN IMPROVED TECHNIQUE [J].
OPFERMANN, J ;
HADRICH, W .
THERMOCHIMICA ACTA, 1995, 263 :29-50
[5]   AN ADVANTAGEOUS VARIANT OF THE OZAWA-FLYNN-WALL ANALYSIS [J].
OPFERMANN, J ;
KAISERSBERGER, E .
THERMOCHIMICA ACTA, 1992, 203 :167-175
[6]  
OPFERMANN J, 1985, RECHENTECHNIK DATENV, V22, P26
[7]  
OPFERMANN J, 1991, THERMISCHE ANALYSENV, P51
[8]  
OPFERMANN J, UNPUB THERMOCHIM ACT
[9]  
OPFERMANN J, 1995, AM LAB FEB, P34
[10]  
Palmour H. III, 1979, SinteringNew Developments. Fourth International Round Table Conference on Sintering, P46