Multiresidue method for determination of organophosphorus pesticides in vegetables

被引：7

作者：

Molinari, GP ^{[1
]}

Cavanna, S ^{[1
]}

Ferroni, B ^{[1
]}

机构：

[1] Fac Agr, Ist Chim Agr & Ambientale, I-29100 Piacenza, Italy

来源：

FOOD ADDITIVES AND CONTAMINANTS | 1998年 / 15卷 / 05期

关键词：

pesticide residues; organophosphate; vegetables; multiresidue method;

D O I：

10.1080/02652039809374675

中图分类号：

O69 [应用化学];

学科分类号：

081704 ;

摘要：

A multiresidue method for the analysis of 14 organophosphorus pesticides has been developed for the rapid control of residues in vegetables before processing. The residues were extracted in ethyl acetate; the extracts were dried purified using an Extrelut 20 column and, after concentration, analysed by gas chromatography with a nitrogen phosphorus detector. Recoveries performed in asparagus, beans, French beans, spinach, peas and zucchini at three fortification levels were over 77% for all pesticides except dementon-S-methyl (70%) and omethoate (52%).

引用

页码：510 / 517

页数：8

共 7 条

[1] AMBRUS A, 1981, J ASSOC OFF ANA CHEM, V64, P733
[2] IUPAC REPORTS ON PESTICIDES .21. APPLICATION OF MULTIRESIDUE PROCEDURES IN PESTICIDES RESIDUES ANALYSIS
AMBRUS, A
THIER, HP
[J]. PURE AND APPLIED CHEMISTRY, 1986, 58 (07) : 1035 - 1062
[3] KADENCZKI L, 1992, J AOAC INT, V75, P53
[4] LUKE AM, 1975, J ASSOC OFF ANA CHEM, V85, P1020
[5] LUKE AM, 1995, AAVV 8 INT C PEST CH, P174
[6] LUKE MA, 1981, J ASSOC OFF ANA CHEM, V64, P1187
[7] LUKE MA, 1988, J ASSOC OFF ANA CHEM, V71, P415

← 1 →