Extraction of polypropylene additives and their analysis by HPLC

被引:41
作者
El Mansouri, H [1 ]
Yagoubi, N [1 ]
Ferrier, D [1 ]
机构
[1] Ctr Etud Pharmaceut, Chim Analyt Lab, F-92296 Chatenay Malabry, France
关键词
column liquid chromatography; polypropylene additives; extraction methods; antioxidants;
D O I
10.1007/BF02466639
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
The polypropylene additives were extracted by dissolution-precipitation and Soxhlet. The Soxhlet method was adapted for the extraction of phosphorous antioxidants. The RP HPLC method with quaternary gradient elution separated five chemical groups of additives: lower molecular mass di-tert-butyl phenol (D.T.B.P.), hindered amine light stabilizers (Tinuvin 326), hindered phenolic antioxidants (Irganox 1010) and phosphorous antioxidants (Irgafos 168 and Ultranox 626) with their degradation products.
引用
收藏
页码:491 / 496
页数:6
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