Preparation of PbS-type PbO nanocrystals in a room-temperature ionic liquid

被引:33
作者
Chen, LJ [1 ]
Zhang, SM
Wu, ZS
Zhang, ZJ
Dang, HX
机构
[1] Henan Univ, Key Lab Special Funct Mat, Kaifeng 475001, Peoples R China
[2] Chinese Acad Sci, Lanzhou Inst Chem Phys, State Key Lab Solid Lubricat, Lanzhou 730000, Peoples R China
关键词
PbS-type PbO nanocrystals; ionic liquid; nanoparticles;
D O I
10.1016/j.matlet.2005.05.031
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
In a strong polar environment of ionic liquid 1-n-butyl-3-ethylimidazolium tetrafluoroborate [BEIM]BF4, PbO nanocrystals with PbS-type crystal structure were successfully synthesized by the thermal decomposition of Pb(OH)(2) at 180 degrees C for 3 h under ambient pressure. The product was characterized by X-ray powder diffraction'(XRD), transmission electron microscopy (TEM), electric diffraction (ED), X-ray photoelectron spectrum (XPS) and elemental analysis. (C) 2005 Elsevier B.V All rights reserved.
引用
收藏
页码:3119 / 3121
页数:3
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