Total synthesis of decumbenine B

被引：42

作者：

Xu, XY ^{[1
]}

Qin, GW ^{[1
]}

Xu, RS ^{[1
]}

Zhu, XZ ^{[1
]}

机构：

[1] Chinese Acad Sci, Shanghai Inst Mat Med, Shanghai 200031, Peoples R China

来源：

TETRAHEDRON | 1998年 / 54卷 / 47期

关键词：

D O I：

10.1016/S0040-4020(98)00894-1

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Decumbenine B, a 3-arylisoquinoline alkaloid isolated from Corydalis decumbens, has been first synthesized from piperonal via 18 steps. The key step was condensation of 5,6-(methylenedioxy)-homophthalic anhydride 5 with Schiff base 6. (C) 1998 Published by Elsevier Science Ltd. All-rights reserved.

引用

页码：14179 / 14188

页数：10

共 18 条

[1] REACTION OF 1,2-DIARYLETHYLAMIDES WITH ETHYL POLYPHOSPHATE (EPP) - CORRELATION OF THE VONBRAUN, RITTER AND BISCHLER-NAPIERALSKI REACTIONS
AGUIRRE, JM
ALESSO, EN
IBANEZ, AF
TOMBARI, DG
IGLESIAS, GYM
[J]. JOURNAL OF HETEROCYCLIC CHEMISTRY, 1989, 26 (01) : 25 - 27
[2] SYNTHETIC STUDIES ON THE LITHIATED TOLUAMIDE-IMINE CYCLO-ADDITION ROUTE TO (+/-)-CORYDALIC ACID METHYL-ESTER
CLARK, RD
JAHANGIR
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1989, 54 (05) : 1174 - 1178
[3] FORMATION OF THE 5-BENZO[D]NAPHTHO[2,3-B]PYRAN SYSTEM DURING AN ATTEMPTED BENZOPHENANTHRIDINE SYNTHESIS
CUSHMAN, M
DIKSHIT, DK
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1980, 45 (25) : 5064 - 5067
[4] TOTAL SYNTHESIS OF (+/-)-CHELIDONINE
CUSHMAN, M
CHOONG, TC
VALKO, JT
KOLECK, MP
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1980, 45 (25) : 5067 - 5073
[5] TOTAL SYNTHESIS OF (+/-)-CORYDALIC ACID METHYL-ESTER
CUSHMAN, M
WONG, WC
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1984, 49 (07) : 1278 - 1280
[6] DESILVA SO, 1978, TETRAHEDRON LETT, V51, P5099
[7] DESILVA SO, 1978, TETRAHEDRON LETT, V51, P5107
[8] DETERMINATION OF THE STEREOCHEMISTRY OF 1-SUBSTITUTED 3-ARYLTETRAHYDROISOQUINOLINES BY H-1-NMR SPECTROSCOPY
DOMINGUEZ, E
LETE, E
BADIA, MD
VILLA, MJ
CASTEDO, L
DOMINGUEZ, D
[J]. TETRAHEDRON, 1987, 43 (08) : 1943 - 1948
[9] HIGHLY STEREOSELECTIVE SYNTHESIS OF 3,4-DIHYDRO-1(2H)-ISOQUINOLINONES AND 8-OXOBERBINES FROM HOMOPHTHALIC ANHYDRIDES AND AZOMETHINES
HAIMOVA, MA
MOLLOV, NM
IVANOVA, SC
DIMITROVA, AI
OGNYANOV, VI
[J]. TETRAHEDRON, 1977, 33 (03) : 331 - 336
[10] HAIMOVA MA, 1971, J CHEM BER, V104, P2601

← 1 2 →