Sonochemical synthesis and characterization of nano-belt lead(II) coordination polymer: New precursor to produce pure phase nano-sized lead(II) oxide

被引：40

作者：

Sadeghzadeh, Homa ^{[1
]}

Morsali, Ali ^{[1
]}

机构：

[1] Tarbiat Modares Univ, Fac Sci, Dept Chem, Tehran, Iran

来源：

ULTRASONICS SONOCHEMISTRY | 2011年 / 18卷 / 01期

关键词：

Nano-particle; Coordination polymer; Lead(II); PbO; COMPLEXES; CDS;

D O I：

10.1016/j.ultsonch.2010.01.011

中图分类号：

O42 [声学];

学科分类号：

070206 ; 082403 ;

摘要：

Nanobelts of new a lead(II) coordination polymer, [Pb(3-pyc)(2)](n) (1), 3-Hpyc = 3-pyridinecarboxilic acid were synthesized by a sonochemical method. The new nano-structure was characterized by scanning electron microscopy, X-ray powder diffraction, elemental analyses and IR spectroscopy. The thermal stability of compound was studied by thermal gravimetric and differential thermal analyses. After calcination of nano-sized compound 1 at 400 degrees C, pure phase nano-sized lead(II) oxide has been produced. (C) 2010 Elsevier B.V. All rights reserved.

引用

页码：80 / 84

页数：5

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