Filming Vitrification with ms Time Resolution

被引:6
作者
Bytchkov, A. [1 ]
Hennet, L. [2 ,3 ]
Pozdnyakova, I. [2 ,3 ]
Wright, J. [1 ]
Vaughan, G. [1 ]
Rossano, S. [4 ]
Madjer, K. [4 ]
Price, D. L. [2 ,3 ]
机构
[1] ESRF, BP 220, F-38043 Grenoble 9, France
[2] Univ Orleans, CEMHTI, F-45071 Orleans 2, France
[3] CEMHTI, F-45071 Orleans 2, France
[4] Univ Marne La Vallee, G2I, F-77454 Marne La Vallee, France
来源
SRI 2009: THE 10TH INTERNATIONAL CONFERENCE ON SYNCHROTRON RADIATION INSTRUMENTATION | 2010年 / 1234卷
关键词
X-ray; scattering; liquid; time-resolved; glass transition;
D O I
10.1063/1.3463177
中图分类号
O59 [应用物理学];
学科分类号
070305 [高分子化学与物理];
摘要
We present X-ray scattering data obtained with the new high temperature setup based on aerodynamic levitation and laser heating. This sample environment has been designed for X-ray scattering experiments up to 3000 degrees C in static and dynamic regimes. X-ray scattering data with good statistics have been recorded during the glass transition of a molten oxide close to an enstatite chondrite composition (Si24AlFe5Mg22Ca16O46) with a 30 ms time resolution. Static measurements on both liquid and glass phases have been also performed with high resolution in both direct and reciprocal spaces.
引用
收藏
页码:219 / +
页数:2
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