Mechanical properties of cellulose fibres and wood.: Orientational aspects in situ investigated with synchrotron radiation

被引:43
作者
Kölln, K
Grotkopp, I
Burghammer, M
Roth, SV
Funari, SS
Dommach, M
Müller, M
机构
[1] Univ Kiel, Inst Expt & Angew Phys, D-24098 Kiel, Germany
[2] European Synchrotron Radiat Facil, F-38043 Grenoble, France
[3] Max Planck Inst Kolloid & Grenzflachenforsch, D-14424 Potsdam, Germany
[4] DESY, HASYLAB, D-22603 Hamburg, Germany
来源
JOURNAL OF SYNCHROTRON RADIATION | 2005年 / 12卷
关键词
X-ray diffraction; cellulose fibres; flax; wood; mechanical properties; tensile strain; strain hardening; orientation distribution;
D O I
10.1107/S0909049505011714
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
Highly oriented native cellulose fibres ( flax) and softwood ( pine) have been investigated by means of X- ray diffraction. Local structural information was obtained by using X- ray microbeams. Tensile tests were performed in situ, revealing a change of orientation of cellulose microfibrils in materials with tensile strain. In flax fibres, the microfibrils rotate during the first percent of stretching, into a more parallel orientation with respect to the fibre axis. For wood, a decrease of orientation with the onset of strain hardening is found for the first time.
引用
收藏
页码:739 / 744
页数:6
相关论文
共 21 条
[1]  
ALEXANDER LE, 1979, XRAY DIFFRACTION MET, pCH4
[2]   The tensile deformation of flax fibres as studied by X-ray scattering [J].
Astley, OM ;
Donald, AM .
JOURNAL OF MATERIALS SCIENCE, 2003, 38 (01) :165-171
[3]  
BURGHAMMER M, 2003, REC RES DEV MACROMOL, V7, P103
[4]  
Cave ID, 1997, WOOD SCI TECHNOL, V31, P143, DOI 10.1007/s002260050023
[5]   CALIBRATION AND CORRECTION OF SPATIAL DISTORTIONS IN 2D DETECTOR SYSTEMS [J].
HAMMERSLEY, AP ;
SVENSSON, SO ;
THOMPSON, A .
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT, 1994, 346 (1-2) :312-321
[6]   SIZE AND ARRANGEMENT OF ELEMENTARY CELLULOSE FIBRILS IN WOOD CELLS - A SMALL-ANGLE X-RAY-SCATTERING STUDY OF PICEA-ABIES [J].
JAKOB, HF ;
FRATZL, P ;
TSCHEGG, SE .
JOURNAL OF STRUCTURAL BIOLOGY, 1994, 113 (01) :13-22
[7]   Cell-wall recovery after irreversible deformation of wood [J].
Keckes, J ;
Burgert, I ;
Frühmann, K ;
Müller, M ;
Kölln, K ;
Hamilton, M ;
Burghammer, M ;
Roth, SV ;
Stanzl-Tschegg, S ;
Fratzl, P .
NATURE MATERIALS, 2003, 2 (12) :810-814
[8]   Imaging of the helical arrangement of cellulose fibrils in wood by synchrotron X-ray microdiffraction [J].
Lichtenegger, H ;
Müller, M ;
Paris, O ;
Riekel, C ;
Fratzl, P .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1999, 32 :1127-1133
[9]  
Lichtenegger H, 1998, MICROFIBRIL ANGLE WO, P140
[10]  
Morton W.E., 1993, PHYS PROPERTIES TEXT