Large cyclic oligomers of furan and acetone. X-ray crystal structure of the hexamer and first synthesis of the nonamer.

被引：16

作者：

Kohnke, FH ^{[1
]}

LaTorre, GL ^{[1
]}

Parisi, MF ^{[1
]}

Menzer, S ^{[1
]}

Williams, DJ ^{[1
]}

机构：

[1] UNIV LONDON IMPERIAL COLL SCI TECHNOL & MED,CHEM CRYSTALLOG LAB,LONDON SW7 2AY,ENGLAND

来源：

TETRAHEDRON LETTERS | 1996年 / 37卷 / 26期

关键词：

D O I：

10.1016/0040-4039(96)00885-4

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

The synthesis of several cyclic oligomers of furan and acetone containing four or more furan units has been re-examined The structure of the [1.(6)](2,5)furanophane C6 has been investigated by X-ray crystallography. The first and efficient synthesis of the [1.(9)](2,5)furanophane C9 is also described. Copyright (C) 1996 Elsevier Science Ltd

引用

页码：4593 / 4596

页数：4

共 15 条

[1] THE CONDENSATION OF METHYL KETONES WITH FURAN [J].

ACKMAN, RG ;

BROWN, WH ;

WRIGHT, GF .

JOURNAL OF ORGANIC CHEMISTRY, 1955, 20 (09) :1147-1158

[2]

CHASTRETTE M, 1988, ORG SYNTH, V6, P856

[3]

DEAN FM, 1984, COMPREHENSIVE HETERO, V4, P542

[4] SIMULATION OF IRREVERSIBLE CYCLIZATION OF BIFUNCTIONAL CHAINS - A COMPUTER-AIDED APPROACH TO THE SYNTHESIS OF MANY-MEMBERED RINGS AND TO THE EVALUATION OF EFFECTIVE MOLARITIES BY PREPARATIVE EXPERIMENTS [J].

ERCOLANI, G ;

MENCARELLI, P .

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2, 1989, (02) :187-191

[5] RING-CLOSURE REACTIONS .28. SYNTHESES OF MANY-MEMBERED RINGS - KINETIC-MODELS FOR THE IRREVERSIBLE CYCLIZATION OF 2 SYMMETRICAL MONOMERS [J].

ERCOLANI, G ;

MANDOLINI, L ;

MENCARELLI, P .

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2, 1990, (05) :747-752

[6] THE STRUCTURE OF OCTAMETHYLTETRAOXAQUATERENE [J].

HAZELL, A .

ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1989, 45 :137-140

[7]

HEALY MD, 1985, J CHEM SOC PERK T 1, P973

[8]

KOBUKE Y, 1976, J AM CHEM SOC, V98, P7474

[9]

KOHNKE FH, 1994, TETRAHEDRON, V50, P9113

[10]

Mandolini L., 1986, ADV PHYS ORG CHEM, V22

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