Size-controlled synthesis of Ru nanoparticles by ethylene glycol reduction

被引:51
作者
Chen, Yong [1 ]
Liew, Kong Yong [1 ]
Li, Jinlin [1 ]
机构
[1] S Cent Univ Nationalieites, Key Lab Catal & Mat Sci State, Ethnic Affairs Commiss & Minist Educ, Wuhan 430074, Hubei Province, Peoples R China
基金
中国国家自然科学基金;
关键词
Ru nanoparticles; size-controlled synthesis; seeding growth; nanomaterials; catalysts;
D O I
10.1016/j.matlet.2007.07.038
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Using two different methods, Ru nanoparticles have been synthesized by chemical reduction of ruthenium nitrosyl nitrate in ethylene glycol using Poly (N-vinyl-2-pyrrolidone) (PVP) as a stabilizer. In a one-step reaction, the average diameters of Ru nanoparticles were controlled in the range of 1.2-6.5 nm with narrow size distributions by changing the synthesis procedure and reaction conditions. In the seeding growth reaction, the Ru nanoparticle size was also precisely controlled by varying the seeds to RU3+ ions ratio, ruthenium particles with different sizes (3.8-7.3 nm) were synthesized. (c) 2007 Elsevier B.V. All rights reserved.
引用
收藏
页码:1018 / 1021
页数:4
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