Space-confined formation of FePt nanoparticles in ordered mesoporous silica SBA-15

被引:55
作者
Kockrick, Emanuel
Krawiec, Piotr
Schnelle, Walter
Geiger, Dorin
Schappacher, Falko M.
Poettgen, Rainer
Kaskel, Stefan
机构
[1] Tech Univ Dresden, Dept Inorgan Chem, D-01662 Dresden, Germany
[2] Max Planck Inst Chem Phys Solids, D-01187 Dresden, Germany
[3] Tech Univ Dresden, Inst Struct Phys, Triebenberg Lab HRTEM & Electron Holograhy, D-01328 Dresden, Germany
[4] Univ Munster, Dept Inorgan & Analyt Chem, D-48149 Munster, Germany
关键词
D O I
10.1002/adma.200601367
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
FePt nanoparticles inside ordered mesoporous silica SBA-15 were synthesized via incipient wetness impregnation and subsequent thermal treatments in reductive atmosphere. The porous matrix is used to prevent sintering and agglomeration during the fcc-FePt to fct-FePt phase transition. According to magnetic measurements and Mossbauer spectroscopic studies, the resulting FePt@SBA-15 composites are ferromagnetic.
引用
收藏
页码:3021 / +
页数:7
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