Low flow, externally air cooled torch for inductively coupled plasma atomic emission spectrometry with axial viewing

被引:12
作者
Hasan, T [1 ]
Praphairaksit, N [1 ]
Houk, RS [1 ]
机构
[1] Iowa State Univ Sci & Technol, Dept Chem, Ames Lab, US Dept Energy, Ames, IA 50011 USA
关键词
inductively coupled plasma (ICP); ICP atomic emission spectrometry (ICP-AES); ICP; torch design; axial viewing; low flow;
D O I
10.1016/S0584-8547(01)00168-9
中图分类号
O433 [光谱学];
学科分类号
0703 ; 070302 ;
摘要
The torch wall is cooled largely by air passing through a cooling jacket added to the outside of a Fassel torch. The plasma is viewed axially through a cooled cone interface centered on the axial channel. The outer argon gas flow can be reduced to 7 l min(-1) with no compromise in performance or torch lifetime. The plasma exhibits the same 'robustness index' and interference effects from Na as the conventional, high-flow ICP supplied with the particular spectrometer used. Detection limits (DL) for lines at similar to 200 nm are poorer by approximately a factor of two, while those for lines at similar to 400 nm are actually better than values typically seen for the same lines by axial viewing of a conventional, high-flow ICP. (C) 2001 Elsevier Science B.V. All rights reserved.
引用
收藏
页码:409 / 418
页数:10
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