Glycol-nitrate combustion synthesis of fine sinter-active yttria

被引：47

作者：

Dasgupta, N ^{[1
]}

Krishnamoorthy, R

Jacob, KT

机构：

[1] Bharat Heavy Elect Ltd, Ceram Technol Inst, Bangalore 560012, Karnataka, India

[2] Indian Inst Sci, Ctr Mat Res, Bangalore 560012, Karnataka, India

[3] Indian Inst Sci, Dept Met, Bangalore 560012, Karnataka, India

来源：

INTERNATIONAL JOURNAL OF INORGANIC MATERIALS | 2001年 / 3卷 / 02期

关键词：

oxides; chemical synthesis; thermogravimetric analysis; electron microscopy; microstructure;

D O I：

10.1016/S1466-6049(00)00108-2

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Yttrium oxide has been synthesized from yttrium nitrate by combustion synthesis using ethylene glycol as the fuel. The combustion characteristics, thermal decomposition, crystallite pattern of the reaction product, and densification of the calcined powders were studied for different glycol/nitrate ratios. The microstructural evolution of the reaction product with increasing calcination temperature was studied. By sintering compacted powders at 1698 K for 7.2 hs. 96% of the theoretical density was achieved. The average grain size was 3 mum and there was no evidence of intra-granular porosity. (C) 2001 Elsevier Science Ltd. All rights: reserved.

引用

页码：143 / 149

页数：7

共 31 条

[1] Synthesis and characterization of MgAl2O4 spinel by PVA evaporation technique [J].

Adak, AK ;

Saha, SK ;

Pramanik, P .

JOURNAL OF MATERIALS SCIENCE LETTERS, 1997, 16 (03) :234-235

[2] PREPARATION AND PROPERTIES OF MONODISPERSED COLLOIDAL PARTICLES OF LANTHANIDE COMPOUNDS .3. YTTRIUM(III) AND MIXED YTTRIUM(III)-CERIUM(III) SYSTEMS [J].

AIKEN, B ;

HSU, WP ;

MATIJEVIC, E .

JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1988, 71 (10) :845-853

[3]

[Anonymous], XRAY DIFFRACTION PRO

[4] Auto ignition synthesis and consolidation of Al2O3-ZrO2 nano/nano composite powders [J].

Bhaduri, S ;

Bhaduri, SB ;

Zhou, E .

JOURNAL OF MATERIALS RESEARCH, 1998, 13 (01) :156-165

[5]

CHICK LA, 1994, NANOSTRUCT MATER, V4, P603, DOI 10.1016/0965-9773(94)90070-1

[6] COMBUSTION SYNTHESIS OF YTTRIA [J].

EKAMBARAM, S ;

PATIL, KC .

JOURNAL OF MATERIALS CHEMISTRY, 1995, 5 (06) :905-908

[7]

FURLONG LR, 1966, AM CERAM SOC BULL, V45, P1051

[8]

GRESKOVICH C, 1973, AM CERAM SOC BULL, V52, P473

[9] Polymerized organic-inorganic synthesis of mixed oxides [J].

Gülgün, MA ;

Nguyen, MH ;

Kriven, WM .

JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1999, 82 (03) :556-560

[10] A NEW APPROACH TO THERMOCHEMICAL CALCULATIONS OF CONDENSED FUEL-OXIDIZER MIXTURES [J].

JAIN, SR ;

ADIGA, KC ;

VERNEKER, VRP .

COMBUSTION AND FLAME, 1981, 40 (01) :71-79

← 1 2 3 4 →