Microwave-assisted syntheses of regioisomerically pure bromorhodamine derivatives

被引:42
作者
Jiao, GS [1 ]
Castro, JC [1 ]
Thoresen, LH [1 ]
Burgess, K [1 ]
机构
[1] Texas A&M Univ, Dept Chem, College Stn, TX 77842 USA
关键词
D O I
10.1021/ol035327u
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
Regioisomerically pure bromo-substituted rhodamine derivatives (bromorosamines) were prepared via microwave-accelerated condensation reactions followed by oxidation with chloranil. Reaction optimization was conveniently performed by monitoring UV absorptions attributed to the product.
引用
收藏
页码:3675 / 3677
页数:3
相关论文
共 8 条
[1]  
BURGESS K, 2000, NEW CHEM BODIPY DYES
[2]   Energy transfer cassettes based on BODIPY® dyes [J].
Burghart, A ;
Thoresen, LH ;
Chen, J ;
Burgess, K ;
Bergström, F ;
Johansson, LBÅ .
CHEMICAL COMMUNICATIONS, 2000, (22) :2203-2204
[3]  
Haugland R.P., 1996, Handbook of Fluorescent Probes and Research Chemicals
[4]   Microwave assisted organic synthesis -: a review [J].
Lidström, P ;
Tierney, J ;
Wathey, B ;
Westman, J .
TETRAHEDRON, 2001, 57 (45) :9225-9283
[5]   Rational design and synthesis of a novel class of highly fluorescent rhodamine dyes that have strong absorption at long wavelengths [J].
Liu, JX ;
Diwu, ZJ ;
Leung, WY ;
Lu, YX ;
Patch, B ;
Haugland, RP .
TETRAHEDRON LETTERS, 2003, 44 (23) :4355-4359
[6]  
MAO F, 1999, Patent No. 15517
[7]   A tentative rationalization of microwave effects in organic synthesis according to the reaction medium, and mechanistic considerations [J].
Perreux, L ;
Loupy, A .
TETRAHEDRON, 2001, 57 (45) :9199-9223
[8]  
ZHANG YZ, 1997, Patent No. 5686261