Improved scalar shift correlation NMR spectroscopy in solids

被引:38
作者
Heindrichs, ASD
Geen, H
Giordani, C
Titman, JJ
机构
[1] Univ Nottingham, Sch Chem, Nottingham NG7 2RD, England
[2] Univ Nottingham, Sch Phys & Astron, Nottingham NG7 2RD, England
基金
英国工程与自然科学研究理事会;
关键词
D O I
10.1016/S0009-2614(01)00018-5
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
New isotropic mixing sequences suitable for scalar correlation experiments in solids have been designed using symmetry principles similar to those employed in the construction of the C7 dipolar recoupling sequence. Compared with existing methods, the new isotropic mixing sequences are appropriate for use with faster MAS rates and show improved magnetization transfer efficiencies For carbon-13. (C) 2001 Elsevier Science B.V. All rights reserved.
引用
收藏
页码:89 / 96
页数:8
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