Analysis by HPLC-MS/MS of biophenolic components in olives and oils

被引:36
作者
Bianco, A
Buiarelli, F
Cartoni, G [1 ]
Coccioli, F
Muzzalupo, I
Polidori, A
Uccella, N
机构
[1] Univ La Sapienza, Dipartimento Chim, I-00185 Rome, Italy
[2] Univ Calabria, CIRASAIA, Mediterranean Agrifood Res, I-87030 Arcavata Di Rende, CS, Italy
关键词
HPLC-MS-/MS; biophenolic compounds; table olive; extra virgin oil;
D O I
10.1081/AL-100103612
中图分类号
O65 [分析化学];
学科分类号
070302 [分析化学]; 081704 [应用化学];
摘要
The aim of this work was to analyze by HPLC-MS-MS natural biophenolic compounds in complex natural samples like olives and olive oils. Eleven benzoic and cinnamic acids, vanillin and other eight biophenolic compounds were studied by liquid chromatography-atmospheric pressure ionization mass spectrometry/mass spectrometry with a Turbo Ion source in the negative mode. To confirm the specific presence. with great sensitivity, of such compounds in olive samples, in brine samples and in extravirgin olive oil the fragmentation of precursor ions into the product species acquisition was used in Multiple Reaction Monitoring (MRM) mode.
引用
收藏
页码:1033 / 1051
页数:19
相关论文
共 17 条
[1]
GC-RIS EVALUATION OF PHENOLIC-COMPOUNDS IN VIRGIN OLIVE OIL [J].
ANGEROSA, F ;
DALESSANDRO, N ;
KONSTANTINOU, P ;
DIGIACINTO, L .
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1995, 43 (07) :1802-1807
[2]
Biophenolic components of olives [J].
Bianco, A ;
Uccella, N .
FOOD RESEARCH INTERNATIONAL, 2000, 33 (06) :475-485
[3]
Comparative investigation of UV, electrochemical and particle beam mass spectrometric detection for the high-performance liquid chromatographic determination of benzoic and cinnamic acids and of their corresponding phenolic acids [J].
Bocchi, C ;
Careri, M ;
Groppi, F ;
Mangia, A ;
Manini, P ;
Mori, G .
JOURNAL OF CHROMATOGRAPHY A, 1996, 753 (02) :157-170
[4]
Liquid chromatographic-mass spectrometric determination of phenolic compounds using a capillary-scale particle beam interface [J].
Cappiello, A ;
Famiglini, G ;
Mangani, F ;
Careri, M ;
Lombardi, P ;
Mucchino, C .
JOURNAL OF CHROMATOGRAPHY A, 1999, 855 (02) :515-527
[5]
Overview of the applications of liquid chromatography mass spectrometry interfacing systems in food analysis: naturally occurring substances in food [J].
Careri, M ;
Mangia, A ;
Musci, M .
JOURNAL OF CHROMATOGRAPHY A, 1998, 794 (1-2) :263-297
[6]
CARTONI GP, 2000, J FOOD SCI, V12, P21
[7]
DeNino A, 1997, J MASS SPECTROM, V32, P533
[8]
Evaluation of high-performance liquid chromatography for determination of phenolic compounds in pear horticultural cultivars [J].
Escarpa, A ;
González, MC .
CHROMATOGRAPHIA, 2000, 51 (1-2) :37-43
[9]
Various applications of liquid chromatography-mass spectrometry to the analysis of phenolic compounds [J].
Pérez-Magariño, S ;
Revilla, I ;
González-SanJosé, ML ;
Beltrán, S .
JOURNAL OF CHROMATOGRAPHY A, 1999, 847 (1-2) :75-81
[10]
Polyphenolic content in five Tuscany cultivars of Olea europaea L. [J].
Romani, A ;
Mulinacci, N ;
Pinelli, P ;
Vincieri, FF ;
Cimato, A .
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1999, 47 (03) :964-967