A novel reduction-oxidation synthetic route to cubic zirconia nanocrystallite

被引：10

作者：

Feng, X ^{[1
]}

Bai, YJ

Lü, B

Zhao, YR

Yang, H

Chi, HR

机构：

[1] Shanghai Univ Sci & Technol, Dept Mech Engn, Jinan 250031, Peoples R China

[2] Qingdao Univ, Coll Mech Engn, Qingdao 266071, Peoples R China

来源：

JOURNAL OF CRYSTAL GROWTH | 2004年 / 262卷 / 1-4期

关键词：

nanostructure; X-ray diffration; crystal morphology; nanomaterials; ceramics; oxides;

D O I：

10.1016/j.jcrysgro.2003.10.063

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

Cubic ZrO2 nanocrystals were successfully synthesized through a novel reduction-oxidation route, in which metal zirconium was reduced from zirconium tetrachloride (ZrCl4) by sodium, and then oxidized in atmosphere. The crystals were characterized by high temperature X-ray powder diffraction and transmission electron microscopy. It was shown that cubic nanocrystalline ZrO2 with high crystallinity was obtained, which consists dominantly of spherical particles with an average size of 17 nm or so. (C) 2003 Elsevier B.V. All rights reserved.

引用

页码：420 / 423

页数：4

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