Determination of enantiomeric excess for amino acid ester salts using FAB mass spectrometry

被引：37

作者：

Sawada, M

Yamaoka, H

Takai, Y

Kawai, Y

Yamada, H

Azuma, T

Fujioka, T

Tanaka, T

机构：

[1] Osaka Univ, Inst Sci & Ind Res, Ctr Mat Anal, Ibaraki, Osaka 567, Japan

[2] Osaka Womens Univ, Dept Nat Sci, Sakai, Osaka 560, Japan

[3] Osaka Inst Technol, Fac Engn, Asahi Ku, Osaka 535, Japan

来源：

CHEMICAL COMMUNICATIONS | 1998年 / 15期

关键词：

D O I：

10.1039/a802029i

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The enantiomeric excess of a-amino acid ester hydrochlorides is determined for the first time using FAB mass spectrometry coupled with enantiomer-labelled host method.

引用

页码：1569 / 1570

页数：2

共 11 条

[1] OPTICAL ISOMER SEPARATION BY LIQUID-CHROMATOGRAPHY [J].

ARMSTRONG, DW .

ANALYTICAL CHEMISTRY, 1987, 59 (02) :A84-&

[2] IDENTIFICATION OF CHIRAL ISOMERS BY FAST ATOM BOMBARDMENT MASS-SPECTROMETRY - DIALKYL TARTRATES [J].

BALDWIN, MA ;

HOWELL, SA ;

WELHAM, KJ ;

WINKLER, FJ .

BIOMEDICAL AND ENVIRONMENTAL MASS SPECTROMETRY, 1988, 16 (1-12) :357-360

[3] CHIRAL AZOPHENOLIC ACERANDS - COLOR INDICATORS TO JUDGE THE ABSOLUTE-CONFIGURATION OF CHIRAL AMINES [J].

KANEDA, T ;

HIROSE, K ;

MISUMI, S .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1989, 111 (02) :742-743

[4] ENANTIOSELECTIVE COMPLEXATION OF CARBOHYDRATE OR CROWN-ETHER HOSTS WITH ORGANIC AMMONIUM ION GUESTS DETECTED BY FAB MASS-SPECTROMETRY [J].

SAWADA, M ;

OKUMURA, Y ;

SHIZUMA, M ;

TAKAI, Y ;

HIDAKA, Y ;

YAMADA, H ;

TANAKA, T ;

KANEDA, T ;

HIROSE, K ;

MISUMI, S ;

TAKAHASHI, S .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1993, 115 (16) :7381-7388

[5] Chiral amino acid recognition detected by electrospray ionization (ESI) and fast atom bombardment (FAB) mass spectrometry (MS) coupled with the enantiomer-labelled (EL) guest method [J].

Sawada, M ;

Takai, Y ;

Yamada, H ;

Nishida, J ;

Kaneda, T ;

Arakawa, R ;

Okamoto, M ;

Hirose, K ;

Tanaka, T ;

Naemura, K .

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2, 1998, (03) :701-710

[6]

Sawada M, 1997, MASS SPECTROM REV, V16, P73

[7] CHIRAL RECOGNITION IN HOST-GUEST COMPLEXATION DETERMINED BY THE ENANTIOMER-LABELED GUEST METHOD USING FAST-ATOM-BOMBARDMENT MASS-SPECTROMETRY [J].

SAWADA, M ;

TAKAI, Y ;

YAMADA, H ;

HIRAYAMA, S ;

KANEDA, T ;

TANAKA, T ;

KAMADA, K ;

MIZOOKU, T ;

TAKEUCHI, S ;

UENO, K ;

HIROSE, K ;

TOBE, Y ;

NAEMURA, K .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1995, 117 (29) :7726-7736

[8]

Sawada M., 1997, J MASS SPECTROM SOC, V45, P439

[9] HOST-GUEST COMPLEXATION .12. TOTAL OPTICAL RESOLUTION OF AMINE AND AMINO ESTER SALTS BY CHROMATOGRAPHY [J].

SOUSA, LR ;

SOGAH, GDY ;

HOFFMAN, DH ;

CRAM, DJ .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1978, 100 (14) :4569-4576

[10]

VOGTLE F, 1980, CHEM ETHERS CROWN 1, pCH2

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