Morphology development of ZnO produced by sonothermal process

被引：6

作者：

Jattukul, Siriprapha ^{[1
]}

Thongtem, Somchai ^{[2
,3
]}

Thongtem, Titipun ^{[1
,3
]}

机构：

[1] Chiang Mai Univ, Dept Chem, Fac Sci, Chiang Mai 50200, Thailand

[2] Chiang Mai Univ, Dept Phys & Mat Sci, Fac Sci, Chiang Mai 50200, Thailand

[3] Chiang Mai Univ, Mat Sci Res Ctr, Fac Sci, Chiang Mai 50200, Thailand

来源：

CERAMICS INTERNATIONAL | 2011年 / 37卷 / 06期

关键词：

Sonothermal reactions; Zinc oxide; Nanoplates in clusters; Nanospears in flower-shaped clusters; Nanorods in clusters; SONOCHEMICAL SYNTHESIS; NANOSTRUCTURES; NANOPARTICLES; TEMPERATURE; NANOROD; GROWTH;

D O I：

10.1016/j.ceramint.2011.02.019

中图分类号：

TQ174 [陶瓷工业]; TB3 [工程材料学];

学科分类号：

081705 [工业催化]; 082905 [生物质能源与材料];

摘要：

Wurtzite ZnO (hcp) was produced by the 80 degrees C sonothermal reactions of 1:5, 1:10, and 1:20 molar ratios of Zn(NO3)(2)center dot 6H(2)O:NaOH in water, containing 2 g, 5 g, 10 g, and 20 g of polyethylene glycol (PEG) with the molecular weights (MWs) of 6000, 10000, and 20000 for 1 h, 3 h, and 5 h. ZnO phase with different morphologies was detected. When the amount of NaOH, both MW and the amount of PEG, and the experimental time were increased, the products still retain their single phase, but their morphologies were changed from nanoplates in clusters to nanospears with sharp tips gathering together in the shape of flowers, and long nanorods with oval tips in clusters. In the present work, formation mechanism of these products was also discussed. (C) 2011 Elsevier Ltd and Techna Group S.r.l. All rights reserved.

引用

页码：2055 / 2059

页数：5

共 23 条

[1]

Syntheses of BaCO3 nanostructures by ultrasonic method [J].